Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids
The work is devoted to the diastereoselective synthesis of 6-aryl-4-methyl-2,8,10-triphenyl-2,3,7-triazaspiro[4,5]deca-3,7-dien-1-ones and 2,4-dimethyl-7,9,11-triaryl-2,4,8-triazaspiro[5,5]undec-8-en-1,3,5-triones by reaction of 1-phenyl-3-methylpyrazolin-5-one and 1,3-dimethylbarbituric acid with c...
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| Дата: | 2005 |
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| Автори: | , , , , |
| Формат: | Стаття |
| Мова: | English |
| Опубліковано: |
НТК «Інститут монокристалів» НАН України
2005
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| Назва видання: | Functional Materials |
| Онлайн доступ: | http://dspace.nbuv.gov.ua/handle/123456789/138861 |
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| Назва журналу: | Digital Library of Periodicals of National Academy of Sciences of Ukraine |
| Цитувати: | Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids / N.N. Kolos, T.V. Beryozkina, F.G. Yaremenko, L.S. Enina, V.I. Musatov // Functional Materials. — 2005. — Т. 12, № 3. — С. 569-576. — Бібліогр.: 7 назв. — англ. |
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irk-123456789-1388612018-06-20T03:09:00Z Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids Kolos, N.N. Beryozkina, T.V. Yaremenko, F.G. Enina, L.S. Musatov, V.I. The work is devoted to the diastereoselective synthesis of 6-aryl-4-methyl-2,8,10-triphenyl-2,3,7-triazaspiro[4,5]deca-3,7-dien-1-ones and 2,4-dimethyl-7,9,11-triaryl-2,4,8-triazaspiro[5,5]undec-8-en-1,3,5-triones by reaction of 1-phenyl-3-methylpyrazolin-5-one and 1,3-dimethylbarbituric acid with chalcones and aromatic aldehydes in the presence of ammonium acetate. The stereochemistry of the compounds obtained has been determined using NOE experiment. Работа посвящена диастереоселективному синтезу 6-арил-4-метил-2,8,10-трифенил-2,3,7-триазаспиро[4,5]дека-3,7-диен-1-онов и 2,4-диметил-7,9,11-триарил-2,4,8-триазаспиро[5,5]ундек-8-ен-1,3,5-трионов в реакциях гетероциклических СН-кислот - 1-фенил-3-метилпиразолин-5-она и 1,3-диметилбарбитуровой кислоты с халконами и ароматическими альдегидами в присутствии ацетата аммония. Стереохимия целевых продуктов определена с помощью NOE-эксперимента. Роботу присвячено дiастереоселективному синтезу 6-арил-4-метил-2,8,10-трифенiл-2,3,7-триазаспiро[4,5]дека-3,7-дiєн-1-онiв та 2,4-диметил-7,9,11-триарил-2,4,8-триазаспiро[5,5]ундец-8-ен-1,3,5-трионiв у реакцiях гетероциклiчних СН-кислот-1-фенiл-3- метилпiразолiн-5-ону та 1,3-диметилбарбiтурової кислоти з халконами та ароматичними альдегiдами у присутностi ацетату амонiю. Стереохiмiю цiльових продуктiв визначено за допомогою NOE-експерименту. 2005 Article Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids / N.N. Kolos, T.V. Beryozkina, F.G. Yaremenko, L.S. Enina, V.I. Musatov // Functional Materials. — 2005. — Т. 12, № 3. — С. 569-576. — Бібліогр.: 7 назв. — англ. 1027-5495 http://dspace.nbuv.gov.ua/handle/123456789/138861 en Functional Materials НТК «Інститут монокристалів» НАН України |
| institution |
Digital Library of Periodicals of National Academy of Sciences of Ukraine |
| collection |
DSpace DC |
| language |
English |
| description |
The work is devoted to the diastereoselective synthesis of 6-aryl-4-methyl-2,8,10-triphenyl-2,3,7-triazaspiro[4,5]deca-3,7-dien-1-ones and 2,4-dimethyl-7,9,11-triaryl-2,4,8-triazaspiro[5,5]undec-8-en-1,3,5-triones by reaction of 1-phenyl-3-methylpyrazolin-5-one and 1,3-dimethylbarbituric acid with chalcones and aromatic aldehydes in the presence of ammonium acetate. The stereochemistry of the compounds obtained has been determined using NOE experiment. |
| format |
Article |
| author |
Kolos, N.N. Beryozkina, T.V. Yaremenko, F.G. Enina, L.S. Musatov, V.I. |
| spellingShingle |
Kolos, N.N. Beryozkina, T.V. Yaremenko, F.G. Enina, L.S. Musatov, V.I. Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids Functional Materials |
| author_facet |
Kolos, N.N. Beryozkina, T.V. Yaremenko, F.G. Enina, L.S. Musatov, V.I. |
| author_sort |
Kolos, N.N. |
| title |
Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids |
| title_short |
Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids |
| title_full |
Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids |
| title_fullStr |
Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids |
| title_full_unstemmed |
Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids |
| title_sort |
diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic ch-acids |
| publisher |
НТК «Інститут монокристалів» НАН України |
| publishDate |
2005 |
| url |
http://dspace.nbuv.gov.ua/handle/123456789/138861 |
| citation_txt |
Diastereoselective synthesis of spirotetrahydropyridines on the basis of heterocyclic CH-acids / N.N. Kolos, T.V. Beryozkina, F.G. Yaremenko, L.S. Enina, V.I. Musatov // Functional Materials. — 2005. — Т. 12, № 3. — С. 569-576. — Бібліогр.: 7 назв. — англ. |
| series |
Functional Materials |
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2023-10-18T21:19:31Z |
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