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Simultaneous thermodynamic and dynamical characterisation using in situ calorimetry with neutron spectroscopy
Both Differential Scanning Calorimetry (DSC) and Quasi-elastic Neutron Scattering (QENS) are powerful analytical tools actively used in studies of phase transitions in complex solid and liquid systems. DSC is typically used to map phase transition temperatures and identify sample states, and QENS p...
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Main Authors: | , , , , , , , |
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Format: | Article |
Language: | English |
Published: |
Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
2019
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Series: | Физика низких температур |
Subjects: | |
Online Access: | http://dspace.nbuv.gov.ua/handle/123456789/175952 |
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Summary: | Both Differential Scanning Calorimetry (DSC) and Quasi-elastic Neutron Scattering (QENS) are powerful
analytical tools actively used in studies of phase transitions in complex solid and liquid systems. DSC is typically used to map phase transition temperatures and identify sample states, and QENS provides information on the
molecular scale dynamical motions, such as molecular self-diffusion or glassy dynamics, associated with such
transitions. Both techniques provide highly valuable complementary information about the sample and in many
cases it would be advantageous to measure in parallel with a view to linking the two observables. The biggest
challenge is that the cell design which differs greatly between the two methods. Here we present a first attempt at
designing a cryogenic system which will allow the simultaneous measurement of calorimetric transitions and
QENS measurements, as tested on the neutron spectrometer IRIS at ISIS neutron scattering facility. The system
temperature range is from 10 K to 300 K. We present and discuss the initial design of the system, preliminary
test results, current challenges and limitations, and future directions. |
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