Microwave assisted synthesis of pyrimido[4,5-d]pyrimidine derivatives in dry media
Pyrimido[4,5-d]pyrimidine derivatives were synthesized by using an efficient, facile and solvent-free procedure. Here, a non-conventional synthetic procedure has been developed where solid support of alumina is used as energy transfer medium under microwave irradiation (MWI) which devoids hazards of...
Збережено в:
| Дата: | 2009 |
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| Автори: | , , , , |
| Формат: | Стаття |
| Мова: | English |
| Опубліковано: |
Інститут молекулярної біології і генетики НАН України
2009
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| Онлайн доступ: | http://dspace.nbuv.gov.ua/handle/123456789/7368 |
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| Назва журналу: | Digital Library of Periodicals of National Academy of Sciences of Ukraine |
| Цитувати: | Microwave assisted synthesis of pyrimido[4,5-d]pyrimidine derivatives in dry media / A.H. Kategaonkar, S.A. Sadaphal, K.F. Shelke, B.B. Shingate, M.S. Shingare // Ukrainica Bioorganica Acta. — 2009. — Т. 7, № 1. — С. 3-7. — Бібліогр.: 19 назв. — англ. |
Репозитарії
Digital Library of Periodicals of National Academy of Sciences of Ukraine| Резюме: | Pyrimido[4,5-d]pyrimidine derivatives were synthesized by using an efficient, facile and solvent-free procedure. Here, a non-conventional synthetic procedure has been developed where solid support of alumina is used as energy transfer medium under microwave irradiation (MWI) which devoids hazards of solution phase reactions. The reaction time has been brought down from minutes to seconds with improved yield as compared to reported method. |
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