Cylindrical magnetron based on the plasmaoptical principles

The operation of any magnetron-type sputtering system is based on using of anomalous glow discharge in a crossed E ┴ B fields. In such systems a principle of magnetic isolation of electrons is realized and idea of magnetic lines equipotentialization for control of ions flow on cathode-target can be...

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Published in:Вопросы атомной науки и техники
Date:2007
Main Authors: Dobrovol's'kii, A.M., Evsyukov, A.N., Goncharov, A.A., Protsenko, I.M.
Format: Article
Language:English
Published: Національний науковий центр «Харківський фізико-технічний інститут» НАН України 2007
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Online Access:https://nasplib.isofts.kiev.ua/handle/123456789/110509
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Cite this:Cylindrical magnetron based on the plasmaoptical principles / A.M. Dobrovol's'kii, A.N. Evsyukov, A.A. Goncharov, I.M. Protsenko // Вопросы атомной науки и техники. — 2007. — № 1. — С. 151-153. — Бібліогр.: 7 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
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author Dobrovol's'kii, A.M.
Evsyukov, A.N.
Goncharov, A.A.
Protsenko, I.M.
author_facet Dobrovol's'kii, A.M.
Evsyukov, A.N.
Goncharov, A.A.
Protsenko, I.M.
citation_txt Cylindrical magnetron based on the plasmaoptical principles / A.M. Dobrovol's'kii, A.N. Evsyukov, A.A. Goncharov, I.M. Protsenko // Вопросы атомной науки и техники. — 2007. — № 1. — С. 151-153. — Бібліогр.: 7 назв. — англ.
collection DSpace DC
container_title Вопросы атомной науки и техники
description The operation of any magnetron-type sputtering system is based on using of anomalous glow discharge in a crossed E ┴ B fields. In such systems a principle of magnetic isolation of electrons is realized and idea of magnetic lines equipotentialization for control of ions flow on cathode-target can be applied quite well. In the present work, with consistent taking these principles into account, the sample of axially-symmetric cylindrical sputtering system of magnetron type is proposed, elaborated and tested. Використання аномального жевріючого розряду в схрещених електричному та магнітному полях є основою функціонування будь-якої магнетронної розпилюючої системи. В таких системах виконується принцип магнітної ізоляції електронів та може бути застосована ідея еквіпотенціалізації магнітних силових ліній з метою керування iонним потоком на катоді-мішені. На основі послідовного використання вказаних плазмооптичних принципів було запропоновано, реалізовано та досліджено варіант аксіально-симетричної циліндричної розпилюючої системи магнетронного типу. Использование аномального тлеющего разряда в скрещенных электрических и магнитных полях является основой функционирования любой магнетронной распылительной системы. В таких системах выполняется принцип магнитной изоляции электронов и может быть применена идея эквипотенциализации магнитных силовых линий для управления ионным потоком на катоде-мишени. На основе последовательного применения указанных плазмооптических принципов предложен, реализован и исследован вариант аксиально-симметричной цилиндрической распылительной системы магнетронного типа.
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fulltext Problems of Atomic Science and Technology. 2007, 1. Series: Plasma Physics (13), p. 151-153 151 CYLINDRICAL MAGNETRON BASED ON THE PLASMAOPTICAL PRINCIPLES A.M. Dobrovol's'kii, A.N. Evsyukov, A.A. Goncharov, I.M. Protsenko Institute of Physics of the National Academy of Sciences of Ukraine, Kiev, Ukraine, e-mail: evsyukov@iop.kiev.ua The operation of any magnetron-type sputtering system is based on using of anomalous glow discharge in a crossed BE ⊥ fields. In such systems a principle of magnetic isolation of electrons is realized and idea of magnetic lines equipotentialization for control of ions flow on cathode-target can be applied quite well. In the present work, with consistent taking these principles into account, the sample of axially-symmetric cylindrical sputtering system of magnetron type is proposed, elaborated and tested. PACS:52.25.Xz,52.27.Aj,52.40.Hf,52.50.Dg,52.75.-d,52.77.-j,52.77.Bn,52.77.Dq,52.80.-s,52.80.Sm,52.80.Vp 1. INTRODUCTION It is hardly possible to imagine the modern plasma technologies of processing of the new exotic materials and functional coatings with given properties without DC and AC magnetron sputtering systems. In spite of the fact that magnetron sputtering systems are known already for a long time and are successfully used in technologies, the sufficient understanding of the physical processes determining their operation is not too clear till now. All such plasmadynamic systems with magnetic isolation of electrons can be divided into two greater classes – planar and cylindrical ones. Cylindrical magnetrons were proposed by Penfold and Thornton in the mid-1970s. The results of investigations of their properties are presented by a lot of references[1- 3]. Both their main advantages and disadvantages are well-known. The operation of any magnetron-type sputtering system is based on use of anomalous glow discharge in a crossed BE ⊥ fields. It is possible to apply plasmaoptics principles, proposed firstly by A.I. Morozov [4,5], to plasmadynamic systems of such types. In the present work, with consistent taking these principles into account, the sample of axially-symmetric cylindrical sputtering system of magnetron type is proposed, elaborated and tested. 2. EXPERIMENTAL CONDITIONS The experiments were carried out at the setup schematically shown in Fig. 1. Cylindrical magnetron sputtering system is placed in the vacuum chamber. There are two opportunities to place samples (4) in the internal magnetron volume: one cylindrical sample directly at the axis or several samples in nosepiece (5). Magnetron has magnetic system (1) assembled on permanent magnets and cooled cathode (2). Cathode is cooled due to thermal contact with reservoir with cold water being pumped through it. Cylindrical cathode made of copper with 59 mm internal diameter, 67 mm outer one and 63 mm height is used. Anode system (3) consists of two moveable units and allows to set different anodes on various depths from outside section of magnetic system at the magnetron axis. It is possible to obtain single anode (when both anode units are connected) or split ones (when there is a gap between the anode units in cathode region localization). Anode electrodes are made of nonmagnetic steel. Usually anode unit has 6 rods located in parallel to working cathode surface and uniformly along a circle. Distance between the anode and the cathode can be adjusted. Besides, single anode rod can be located exactly at the magnetron axis. Working gas (argon) is supplied directly into the chamber and produces working pressure from 10-5 up to 10-2 Torr. Magnetron magnetic system forms axially symmetric magnetic field (see Fig. 2). The magnetic system boundaries are shown by solid parallel line (3) in this figure. Rectangles (1) show cathode localization. Anodes localization are shown by rectangles (2). The configuration of magnetic field lines provides formation of magnetic trap for electrons above the cathode surface and magnetic insulation from the anodes. Magnetic field value at the axis of system is about 0.065 T, and one nearby the cathode surface – 0.075 T. Magnetron magnetic field lines were calculated as lines of equal magnetic flux ( =const). The magnetic flux values were evaluated from magnitudes of magnetic field BZ accordingly to the following equation: . 2 1 zr Bz ∂ ∂ ⋅ ⋅ = ψ π Photographs of discharges were made in case of absence of bottom anode module by digital camera. Fig. 1. Principle scheme of the experiments with magnetron type sputtering system. 1-magnetic system; 2-cathode;3-anode; 4-sample;5-samples holder mailto:evsyukov@iop.kiev.ua 152 The physical processes determining behavior of this sputtering system can be close to plasma accelerator with closed electron drift and extended acceleration zone [6]. 3. RESULTS In our experiments plasmaoptical magnetron operated in two modes corresponding to the different types of discharges. The photos of this discharge are shown in Fig.3. It is possible to achieve these regimes by pressure increase. Dependencies of discharge voltage and current via pressure are presented on Fig. 4. The first discharge mode is characterized by low current (up to 100 mA). The upper limit of existence of this mode is correlated with plasmadynamic and geometric parameters (e.g. breakdown voltage, cathode surface cleanness, cathode-anode distance) and is about 3·10-3 Torr. During pressure increase the current value and the luminescence intensity are growing. The second discharge mode is characterized by high current (up to 2 A in our experiments) and high luminescence intensity. Switch to this mode occurrs in spurts with change of discharge color from blue to green. The bottom limit of existence of this magnetron discharge mode is correlated with plasmadynamic and geometric parameters too and is about 5·10-3 Torr. During pressure increase the current value and the luminescence intensity are growing. As one can see from Fig. 4, curve 1 conforms to the first discharge regime in all pressure range. Thus magnetron discharge regime has both pressure and breakdown voltage limits. One can see from Fig. 2 that in the central part of the cathode region magnetic field lines extend in parallel enough way to the cathode surface. Use of split anodes leads to formation of virtual ones along these lines. In this case we have the treatment of all cathode surface without anode shadows on samples surface. Experiments show that the magnetron continues its normal operation up to virtual anode size of 55 mm. Cathode surface inspection after the sputtering test shows the whole cathode surface etching with more intensive zone in the central plane (about 60% width relatively to total cathode height). Considering ions arriving to the cathode surface from edge of plasma positive column in accordance with well- known formula we can calculate the density of charged particles for high-current mode the discharge: ,24.0,)1( i e iiiC M Tknejjj ⋅⋅ ⋅⋅⋅=⋅+= γ where jC- current density on cathode ( j c= I d SC , SC - cathode square), ji- ions current density, - secondary electron emission coefficient (is about 0.1), ni- ions density, Mi- ion mass (Ar), Te- electron temperature. Thus ions density is about 1.54x1013 cm-3. Ionization degree in this system is higher than that in typical magnetron and is about 8 %. We suppose that electron temperature is about 20 eV. Under conditions of our experiments in high-current operation mode deposition rate was about 500 nm/min. Taking into consideration ion current density and deposition rate we can estimate a sputter yield Y: Fig. 2. Magnetron magnetic field lines ( Wb) 1-cathodes; 2-anodes; 3-magnetic system boundaries Fig. 3. Photos of discharges in different modes. 1 - P=3x10-3 Torr, Id=40mA, Ud=2000V; 2 - P=6x10-3 Torr, Id=1.25A, Ud=400V 153 17.13 = ⋅ ⋅ = ija eDY , where D – deposition rate, a - identity parameter (2.2 Å for copper). We can suppose that argon ion energy is about 350 eV [7]. That fact confirms existence of cathode potential drop and plasma positive column in region of the anodes. Plasmaoptical principles suggest virtual anode existence. These principles require a presence of magnetized electrons and nonmagnetized ions. These criterion can be written as ,, LrLr ie <> where re and ri – are Larmor radii of electron and ion correspondingly, L – cathode-anode distance ( 10 mm). On high-current mode for fast electrons in cathode region (Te 350 eV) and for slow ions in plasma positive column (Ti 20 eV) we can write r e 1mm ,ri 60mm , L 10mm. As one can see the necessary conditions for plasmaoptical principles are created and existence of virtual anode is experimentally confirmed. CONCLUSIONS We describe a consistent application of plasmaoptical principles of magnetic isolation and equipotentialization of magnetic field lines for creation of sputtering system magnetron type. We carried out tests and some preliminary investigations of its operation. Discharge in cylindrical magnetron with strong magnetic field in the whole volume has two main stages. Transition between the discharge stages happens in spurts. High-current stage is characterized by abrupt voltage reduction with current growth in spurts and weak dependence of working voltage on pressure. Anode to cathode distance and the anode localization determine some peculiarities of the magnetron operation. Efficient high-current discharge glow is possible in the pressure range from 5x10-3 Torr. Preliminary sample preparation before sputtering is possible immediately in this magnetron. In our experiments high-current mode allows to achieve sputtering rate from copper target of about 500 nm/min. REFERENCES 1. J.A.Thornton, A.S. Penfold. Thin Film Processes. New York:”Academic Press”,1978. 2 D.A. Glocker, M.M. Romach, V.W. Lindberg. Recent developments in inverted cylindrical magnetron sputtering // Surface and Coating Technol. 2001, v.146-147, p. 457-462. 3. M. Amberg, J. Geerk, M. Keller, A. Fischer. Desing, characterisation and operation of an inverted cylindrical magnetron for metal deposition // Plasma Devices and Operations. 2004, v.12, N 3, p. 175-186. 4. A.I. Morozov. Focusing of Cold Quasineutral Beams in Electromagnetic Fields // Soviet Physics – Doklady. 1966, v10, N8, p.775-777. 5. A. Morozov and S. Lebedev. Reviews of Plasma Physics / ed. by M. Leontovich. New York: “Consultants Bureau”, 1975. 6. A.I. Morozov, Yu.V. Esinchuk, G.N. Tilinin, A.V.Trofimov, Yu.A.Shchepkin. Plasma Accelerator with Closed Electron Drift and Extended Acceleration Zone // Soviet Physics Technical Physics. 1972, v.17, p. 38. 7. H. Coufal, H.F. Winter and H.L. Bay. Energy transfer from noble-gas ions to surfaces: Collision with carbon, silicon, copper, silver, and gold in the range 100- 4000 eV // Phys. Rev. B. 1991, v.44, N10, p. 4747. . , . , . , . . . , - . . , . , . , . . i . , . Fig. 4. Dependencies of discharge voltage [Ud](solid lines) and current [Id](dash lines) on pressure at different maximum discharge power: 1 – 0.5 W; 2 – 300W; 3 – 600W; 4 - 900W
id nasplib_isofts_kiev_ua-123456789-110509
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
issn 1562-6016
language English
last_indexed 2025-12-07T15:45:24Z
publishDate 2007
publisher Національний науковий центр «Харківський фізико-технічний інститут» НАН України
record_format dspace
spelling Dobrovol's'kii, A.M.
Evsyukov, A.N.
Goncharov, A.A.
Protsenko, I.M.
2017-01-04T17:23:01Z
2017-01-04T17:23:01Z
2007
Cylindrical magnetron based on the plasmaoptical principles / A.M. Dobrovol's'kii, A.N. Evsyukov, A.A. Goncharov, I.M. Protsenko // Вопросы атомной науки и техники. — 2007. — № 1. — С. 151-153. — Бібліогр.: 7 назв. — англ.
1562-6016
https://nasplib.isofts.kiev.ua/handle/123456789/110509
PACS:52.25.Xz,52.27.Aj,52.40.Hf,52.50.Dg,52.75.-d,52.77.-j,52.77.Bn,52.77.Dq,52.80.-s,52.80.Sm,52.80.Vp
The operation of any magnetron-type sputtering system is based on using of anomalous glow discharge in a crossed E ┴ B fields. In such systems a principle of magnetic isolation of electrons is realized and idea of magnetic lines equipotentialization for control of ions flow on cathode-target can be applied quite well. In the present work, with consistent taking these principles into account, the sample of axially-symmetric cylindrical sputtering system of magnetron type is proposed, elaborated and tested.
Використання аномального жевріючого розряду в схрещених електричному та магнітному полях є основою функціонування будь-якої магнетронної розпилюючої системи. В таких системах виконується принцип магнітної ізоляції електронів та може бути застосована ідея еквіпотенціалізації магнітних силових ліній з метою керування iонним потоком на катоді-мішені. На основі послідовного використання вказаних плазмооптичних принципів було запропоновано, реалізовано та досліджено варіант аксіально-симетричної циліндричної розпилюючої системи магнетронного типу.
Использование аномального тлеющего разряда в скрещенных электрических и магнитных полях является основой функционирования любой магнетронной распылительной системы. В таких системах выполняется принцип магнитной изоляции электронов и может быть применена идея эквипотенциализации магнитных силовых линий для управления ионным потоком на катоде-мишени. На основе последовательного применения указанных плазмооптических принципов предложен, реализован и исследован вариант аксиально-симметричной цилиндрической распылительной системы магнетронного типа.
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Національний науковий центр «Харківський фізико-технічний інститут» НАН України
Вопросы атомной науки и техники
Low temperature plasma and plasma technologies
Cylindrical magnetron based on the plasmaoptical principles
Циліндричний магнетрон на принципах плазмооптики
Цилиндрический магнетрон на принципах плазмооптики
Article
published earlier
spellingShingle Cylindrical magnetron based on the plasmaoptical principles
Dobrovol's'kii, A.M.
Evsyukov, A.N.
Goncharov, A.A.
Protsenko, I.M.
Low temperature plasma and plasma technologies
title Cylindrical magnetron based on the plasmaoptical principles
title_alt Циліндричний магнетрон на принципах плазмооптики
Цилиндрический магнетрон на принципах плазмооптики
title_full Cylindrical magnetron based on the plasmaoptical principles
title_fullStr Cylindrical magnetron based on the plasmaoptical principles
title_full_unstemmed Cylindrical magnetron based on the plasmaoptical principles
title_short Cylindrical magnetron based on the plasmaoptical principles
title_sort cylindrical magnetron based on the plasmaoptical principles
topic Low temperature plasma and plasma technologies
topic_facet Low temperature plasma and plasma technologies
url https://nasplib.isofts.kiev.ua/handle/123456789/110509
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