Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy

Raman spectra of KTa₀.₅Nb₀.₅O₃ nanopowder solid solution were obtained at the temperatures from –190°C to 600°C and investigated for the first time. The compound was synthesized by a new technology. Temperature dependences of the intensity, width and frequency of the B₁(TO₂), A₁(TO₁), B₁(TO₃), A₁(TO...

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Published in:Functional Materials
Date:2013
Main Authors: Golovina, I.S., Bryksa, V.P., Strelchuk, V.V., Geifman, I.N.
Format: Article
Language:English
Published: НТК «Інститут монокристалів» НАН України 2013
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Online Access:https://nasplib.isofts.kiev.ua/handle/123456789/119908
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Journal Title:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Cite this:Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy / I.S. Golovina, V.P. Bryksa, V.V. Strelchuk, I.N. Geifman // Functional Materials. — 2013. — Т. 20, № 1. — С. 75-80. — Бібліогр.: 20 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
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author Golovina, I.S.
Bryksa, V.P.
Strelchuk, V.V.
Geifman, I.N.
author_facet Golovina, I.S.
Bryksa, V.P.
Strelchuk, V.V.
Geifman, I.N.
citation_txt Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy / I.S. Golovina, V.P. Bryksa, V.V. Strelchuk, I.N. Geifman // Functional Materials. — 2013. — Т. 20, № 1. — С. 75-80. — Бібліогр.: 20 назв. — англ.
collection DSpace DC
container_title Functional Materials
description Raman spectra of KTa₀.₅Nb₀.₅O₃ nanopowder solid solution were obtained at the temperatures from –190°C to 600°C and investigated for the first time. The compound was synthesized by a new technology. Temperature dependences of the intensity, width and frequency of the B₁(TO₂), A₁(TO₁), B₁(TO₃), A₁(TO₃) and B₂(TO₃) modes are thoroughly analyzed. A significant expanding of the temperature ranges of all phase transitions, correlated with a spread of particle sizes is registered. It was found that an average temperature of each of the phase transitions is shifted in different way, in particular: a low-temperature transition at 30 degrees higher, the middle transition at 10 degrees higher, and the ferroelectric phase transition occurs at 20 degrees lower than the temperature of the corresponding transitions in single-crystal KTa₀.₅Nb₀.₅O₃.
first_indexed 2025-12-07T21:05:16Z
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last_indexed 2025-12-07T21:05:16Z
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publisher НТК «Інститут монокристалів» НАН України
record_format dspace
spelling Golovina, I.S.
Bryksa, V.P.
Strelchuk, V.V.
Geifman, I.N.
2017-06-10T11:04:06Z
2017-06-10T11:04:06Z
2013
Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy / I.S. Golovina, V.P. Bryksa, V.V. Strelchuk, I.N. Geifman // Functional Materials. — 2013. — Т. 20, № 1. — С. 75-80. — Бібліогр.: 20 назв. — англ.
1027-5495
DOI: dx.doi.org/10.15407/fm20.01.075
https://nasplib.isofts.kiev.ua/handle/123456789/119908
Raman spectra of KTa₀.₅Nb₀.₅O₃ nanopowder solid solution were obtained at the temperatures from –190°C to 600°C and investigated for the first time. The compound was synthesized by a new technology. Temperature dependences of the intensity, width and frequency of the B₁(TO₂), A₁(TO₁), B₁(TO₃), A₁(TO₃) and B₂(TO₃) modes are thoroughly analyzed. A significant expanding of the temperature ranges of all phase transitions, correlated with a spread of particle sizes is registered. It was found that an average temperature of each of the phase transitions is shifted in different way, in particular: a low-temperature transition at 30 degrees higher, the middle transition at 10 degrees higher, and the ferroelectric phase transition occurs at 20 degrees lower than the temperature of the corresponding transitions in single-crystal KTa₀.₅Nb₀.₅O₃.
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НТК «Інститут монокристалів» НАН України
Functional Materials
Characterization and properties
Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy
Article
published earlier
spellingShingle Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy
Golovina, I.S.
Bryksa, V.P.
Strelchuk, V.V.
Geifman, I.N.
Characterization and properties
title Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy
title_full Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy
title_fullStr Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy
title_full_unstemmed Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy
title_short Phase transitions in the nanopowders KTa₀.₅Nb₀.₅O₃ studied by Raman spectroscopy
title_sort phase transitions in the nanopowders kta₀.₅nb₀.₅o₃ studied by raman spectroscopy
topic Characterization and properties
topic_facet Characterization and properties
url https://nasplib.isofts.kiev.ua/handle/123456789/119908
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AT geifmanin phasetransitionsinthenanopowderskta05nb05o3studiedbyramanspectroscopy