Diamond microcrystallites formation through the phase transition graphite→liquid→diamond

The paper presents the results of synthesizing the diamond microparticles (3 to 5 µm) in a spark discharge in hydrogen at the low pressure (100 Torr). The obtained growth rate ~5 µm/s is uniquely high. Our analysis of the nature of particles by using SEM and Raman spectroscopy demonstrates that thes...

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Veröffentlicht in:Semiconductor Physics Quantum Electronics & Optoelectronics
Datum:2006
1. Verfasser: Semikina, T.V.
Format: Artikel
Sprache:Englisch
Veröffentlicht: Інститут фізики напівпровідників імені В.Є. Лашкарьова НАН України 2006
Online Zugang:https://nasplib.isofts.kiev.ua/handle/123456789/121583
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Zitieren:Diamond microcrystallites formation through the phase transition graphite→liquid→diamond / T.V. Semikina // Semiconductor Physics Quantum Electronics & Optoelectronics. — 2006. — Т. 8, № 1. — С. 22-28. — Бібліогр.: 19 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
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author Semikina, T.V.
author_facet Semikina, T.V.
citation_txt Diamond microcrystallites formation through the phase transition graphite→liquid→diamond / T.V. Semikina // Semiconductor Physics Quantum Electronics & Optoelectronics. — 2006. — Т. 8, № 1. — С. 22-28. — Бібліогр.: 19 назв. — англ.
collection DSpace DC
container_title Semiconductor Physics Quantum Electronics & Optoelectronics
description The paper presents the results of synthesizing the diamond microparticles (3 to 5 µm) in a spark discharge in hydrogen at the low pressure (100 Torr). The obtained growth rate ~5 µm/s is uniquely high. Our analysis of the nature of particles by using SEM and Raman spectroscopy demonstrates that these particles are cubic high quality diamond. Using the result of SIM images after cross-cutting of the sample by FIB, it is concluded that diamond does not grow on the substrate and running process is not CVD. Discussing the theory of the spark discharge, it is suggested that the process occurs at high pressures and temperatures. A hypothesis of diamond formation through a diffusion mechanism of the direct phase transition is presented.
first_indexed 2025-11-25T06:43:45Z
format Article
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id nasplib_isofts_kiev_ua-123456789-121583
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
issn 1560-8034
language English
last_indexed 2025-11-25T06:43:45Z
publishDate 2006
publisher Інститут фізики напівпровідників імені В.Є. Лашкарьова НАН України
record_format dspace
spelling Semikina, T.V.
2017-06-14T17:15:51Z
2017-06-14T17:15:51Z
2006
Diamond microcrystallites formation through the phase transition graphite→liquid→diamond / T.V. Semikina // Semiconductor Physics Quantum Electronics & Optoelectronics. — 2006. — Т. 8, № 1. — С. 22-28. — Бібліогр.: 19 назв. — англ.
1560-8034
PACS 81.05.Uw
https://nasplib.isofts.kiev.ua/handle/123456789/121583
The paper presents the results of synthesizing the diamond microparticles (3 to 5 µm) in a spark discharge in hydrogen at the low pressure (100 Torr). The obtained growth rate ~5 µm/s is uniquely high. Our analysis of the nature of particles by using SEM and Raman spectroscopy demonstrates that these particles are cubic high quality diamond. Using the result of SIM images after cross-cutting of the sample by FIB, it is concluded that diamond does not grow on the substrate and running process is not CVD. Discussing the theory of the spark discharge, it is suggested that the process occurs at high pressures and temperatures. A hypothesis of diamond formation through a diffusion mechanism of the direct phase transition is presented.
The author wish to thank Dr Y. Takagi for opening up
 the opportunities to work in the research group in the
 Department of Environmental and Materials Science,
 Teikyo University of Science & Technology, Japan as
 well as for technical supporting the experiments. The
 author thanks students T. Hirai and T. Kawai for their
 assistance and collaboration in the common
 experimental work for growing the diamonds. The
 author also thanks Dr A.I. Kutsay (Institute of Superhard
 Materials, NANU, Kiev), M.G. Dusheyko and
 Yu.V. Yasievich (National Technical University of
 Ukraine “KPI”, Kiev) and Professor V.G. Litovchenko
 (Institute of Semiconductor Physics, NANU, Kiev) for
 the discussion of some parts of this work.
en
Інститут фізики напівпровідників імені В.Є. Лашкарьова НАН України
Semiconductor Physics Quantum Electronics & Optoelectronics
Diamond microcrystallites formation through the phase transition graphite→liquid→diamond
Article
published earlier
spellingShingle Diamond microcrystallites formation through the phase transition graphite→liquid→diamond
Semikina, T.V.
title Diamond microcrystallites formation through the phase transition graphite→liquid→diamond
title_full Diamond microcrystallites formation through the phase transition graphite→liquid→diamond
title_fullStr Diamond microcrystallites formation through the phase transition graphite→liquid→diamond
title_full_unstemmed Diamond microcrystallites formation through the phase transition graphite→liquid→diamond
title_short Diamond microcrystallites formation through the phase transition graphite→liquid→diamond
title_sort diamond microcrystallites formation through the phase transition graphite→liquid→diamond
url https://nasplib.isofts.kiev.ua/handle/123456789/121583
work_keys_str_mv AT semikinatv diamondmicrocrystallitesformationthroughthephasetransitiongraphiteliquiddiamond