Influence of the liquid helium meniscus on neutron reflectometry data

Neutron reflectometry offers a unique opportunity for the direct observation of nanostratification in ³He–⁴He
 mixtures in the ultra-low temperature limit. Unfortunately the results of recent experiments could not be wellmodelled
 on account of a seemingly anomalous variation of refl...

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Опубліковано в: :Физика низких температур
Дата:2016
Автори: Kinane, C.J., Kirichek, O., Charlton, T.R., McClintock, P.V.E.
Формат: Стаття
Мова:Англійська
Опубліковано: Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України 2016
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Онлайн доступ:https://nasplib.isofts.kiev.ua/handle/123456789/128468
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Цитувати:Influence of the liquid helium meniscus on neutron reflectometry data / C.J. Kinane, O. Kirichek, T.R. Charlton,P.V.E. McClintock // Физика низких температур. — 2016. — Т. 42, № 2. — С. 202–206. — Бібліогр.: 24 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
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author Kinane, C.J.
Kirichek, O.
Charlton, T.R.
McClintock, P.V.E.
author_facet Kinane, C.J.
Kirichek, O.
Charlton, T.R.
McClintock, P.V.E.
citation_txt Influence of the liquid helium meniscus on neutron reflectometry data / C.J. Kinane, O. Kirichek, T.R. Charlton,P.V.E. McClintock // Физика низких температур. — 2016. — Т. 42, № 2. — С. 202–206. — Бібліогр.: 24 назв. — англ.
collection DSpace DC
container_title Физика низких температур
description Neutron reflectometry offers a unique opportunity for the direct observation of nanostratification in ³He–⁴He
 mixtures in the ultra-low temperature limit. Unfortunately the results of recent experiments could not be wellmodelled
 on account of a seemingly anomalous variation of reflectivity with momentum transfer. We now hypothesize
 that this effect is attributable to an optical distortion caused by the liquid’s meniscus near the container
 wall. The validity of this idea is tested and confirmed through a subsidiary experiment on a D₂O sample, showing
 that the meniscus can significantly distort results if the beam size in the horizontal plane is comparable with,
 or bigger than, the diameter of the container. The meniscus problem can be eliminated if the beam size is substantially
 smaller than the diameter of the container, such that reflection takes place only from the flat region of
 the liquid surface thus excluding the meniscus tails. Practical measures for minimizing the meniscus distortion
 effect are discussed.
first_indexed 2025-12-07T21:14:38Z
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last_indexed 2025-12-07T21:14:38Z
publishDate 2016
publisher Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
record_format dspace
spelling Kinane, C.J.
Kirichek, O.
Charlton, T.R.
McClintock, P.V.E.
2018-01-09T16:31:53Z
2018-01-09T16:31:53Z
2016
Influence of the liquid helium meniscus on neutron reflectometry data / C.J. Kinane, O. Kirichek, T.R. Charlton,P.V.E. McClintock // Физика низких температур. — 2016. — Т. 42, № 2. — С. 202–206. — Бібліогр.: 24 назв. — англ.
0132-6414
PACS: 61.05.F–
https://nasplib.isofts.kiev.ua/handle/123456789/128468
Neutron reflectometry offers a unique opportunity for the direct observation of nanostratification in ³He–⁴He
 mixtures in the ultra-low temperature limit. Unfortunately the results of recent experiments could not be wellmodelled
 on account of a seemingly anomalous variation of reflectivity with momentum transfer. We now hypothesize
 that this effect is attributable to an optical distortion caused by the liquid’s meniscus near the container
 wall. The validity of this idea is tested and confirmed through a subsidiary experiment on a D₂O sample, showing
 that the meniscus can significantly distort results if the beam size in the horizontal plane is comparable with,
 or bigger than, the diameter of the container. The meniscus problem can be eliminated if the beam size is substantially
 smaller than the diameter of the container, such that reflection takes place only from the flat region of
 the liquid surface thus excluding the meniscus tails. Practical measures for minimizing the meniscus distortion
 effect are discussed.
We thank the ISIS sample environment group for valuable
 technical assistance. This work was supported by the
 EPSRC grant EP/F021429/1 “Critical and surface phenomena
 of quantum fluids”.
en
Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
Физика низких температур
Морфология и свойства наноструктур
Influence of the liquid helium meniscus on neutron reflectometry data
Article
published earlier
spellingShingle Influence of the liquid helium meniscus on neutron reflectometry data
Kinane, C.J.
Kirichek, O.
Charlton, T.R.
McClintock, P.V.E.
Морфология и свойства наноструктур
title Influence of the liquid helium meniscus on neutron reflectometry data
title_full Influence of the liquid helium meniscus on neutron reflectometry data
title_fullStr Influence of the liquid helium meniscus on neutron reflectometry data
title_full_unstemmed Influence of the liquid helium meniscus on neutron reflectometry data
title_short Influence of the liquid helium meniscus on neutron reflectometry data
title_sort influence of the liquid helium meniscus on neutron reflectometry data
topic Морфология и свойства наноструктур
topic_facet Морфология и свойства наноструктур
url https://nasplib.isofts.kiev.ua/handle/123456789/128468
work_keys_str_mv AT kinanecj influenceoftheliquidheliummeniscusonneutronreflectometrydata
AT kiricheko influenceoftheliquidheliummeniscusonneutronreflectometrydata
AT charltontr influenceoftheliquidheliummeniscusonneutronreflectometrydata
AT mcclintockpve influenceoftheliquidheliummeniscusonneutronreflectometrydata