Influence of the liquid helium meniscus on neutron reflectometry data

Neutron reflectometry offers a unique opportunity for the direct observation of nanostratification in ³He–⁴He mixtures in the ultra-low temperature limit. Unfortunately the results of recent experiments could not be wellmodelled on account of a seemingly anomalous variation of reflectivity with mo...

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Опубліковано в: :Физика низких температур
Дата:2016
Автори: Kinane, C.J., Kirichek, O., Charlton, T.R., McClintock, P.V.E.
Формат: Стаття
Мова:English
Опубліковано: Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України 2016
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Онлайн доступ:https://nasplib.isofts.kiev.ua/handle/123456789/128468
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Назва журналу:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Цитувати:Influence of the liquid helium meniscus on neutron reflectometry data / C.J. Kinane, O. Kirichek, T.R. Charlton,P.V.E. McClintock // Физика низких температур. — 2016. — Т. 42, № 2. — С. 202–206. — Бібліогр.: 24 назв. — англ.

Репозитарії

Digital Library of Periodicals of National Academy of Sciences of Ukraine
id nasplib_isofts_kiev_ua-123456789-128468
record_format dspace
spelling Kinane, C.J.
Kirichek, O.
Charlton, T.R.
McClintock, P.V.E.
2018-01-09T16:31:53Z
2018-01-09T16:31:53Z
2016
Influence of the liquid helium meniscus on neutron reflectometry data / C.J. Kinane, O. Kirichek, T.R. Charlton,P.V.E. McClintock // Физика низких температур. — 2016. — Т. 42, № 2. — С. 202–206. — Бібліогр.: 24 назв. — англ.
0132-6414
PACS: 61.05.F–
https://nasplib.isofts.kiev.ua/handle/123456789/128468
Neutron reflectometry offers a unique opportunity for the direct observation of nanostratification in ³He–⁴He mixtures in the ultra-low temperature limit. Unfortunately the results of recent experiments could not be wellmodelled on account of a seemingly anomalous variation of reflectivity with momentum transfer. We now hypothesize that this effect is attributable to an optical distortion caused by the liquid’s meniscus near the container wall. The validity of this idea is tested and confirmed through a subsidiary experiment on a D₂O sample, showing that the meniscus can significantly distort results if the beam size in the horizontal plane is comparable with, or bigger than, the diameter of the container. The meniscus problem can be eliminated if the beam size is substantially smaller than the diameter of the container, such that reflection takes place only from the flat region of the liquid surface thus excluding the meniscus tails. Practical measures for minimizing the meniscus distortion effect are discussed.
We thank the ISIS sample environment group for valuable technical assistance. This work was supported by the EPSRC grant EP/F021429/1 “Critical and surface phenomena of quantum fluids”.
en
Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
Физика низких температур
Морфология и свойства наноструктур
Influence of the liquid helium meniscus on neutron reflectometry data
Article
published earlier
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
title Influence of the liquid helium meniscus on neutron reflectometry data
spellingShingle Influence of the liquid helium meniscus on neutron reflectometry data
Kinane, C.J.
Kirichek, O.
Charlton, T.R.
McClintock, P.V.E.
Морфология и свойства наноструктур
title_short Influence of the liquid helium meniscus on neutron reflectometry data
title_full Influence of the liquid helium meniscus on neutron reflectometry data
title_fullStr Influence of the liquid helium meniscus on neutron reflectometry data
title_full_unstemmed Influence of the liquid helium meniscus on neutron reflectometry data
title_sort influence of the liquid helium meniscus on neutron reflectometry data
author Kinane, C.J.
Kirichek, O.
Charlton, T.R.
McClintock, P.V.E.
author_facet Kinane, C.J.
Kirichek, O.
Charlton, T.R.
McClintock, P.V.E.
topic Морфология и свойства наноструктур
topic_facet Морфология и свойства наноструктур
publishDate 2016
language English
container_title Физика низких температур
publisher Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
format Article
description Neutron reflectometry offers a unique opportunity for the direct observation of nanostratification in ³He–⁴He mixtures in the ultra-low temperature limit. Unfortunately the results of recent experiments could not be wellmodelled on account of a seemingly anomalous variation of reflectivity with momentum transfer. We now hypothesize that this effect is attributable to an optical distortion caused by the liquid’s meniscus near the container wall. The validity of this idea is tested and confirmed through a subsidiary experiment on a D₂O sample, showing that the meniscus can significantly distort results if the beam size in the horizontal plane is comparable with, or bigger than, the diameter of the container. The meniscus problem can be eliminated if the beam size is substantially smaller than the diameter of the container, such that reflection takes place only from the flat region of the liquid surface thus excluding the meniscus tails. Practical measures for minimizing the meniscus distortion effect are discussed.
issn 0132-6414
url https://nasplib.isofts.kiev.ua/handle/123456789/128468
citation_txt Influence of the liquid helium meniscus on neutron reflectometry data / C.J. Kinane, O. Kirichek, T.R. Charlton,P.V.E. McClintock // Физика низких температур. — 2016. — Т. 42, № 2. — С. 202–206. — Бібліогр.: 24 назв. — англ.
work_keys_str_mv AT kinanecj influenceoftheliquidheliummeniscusonneutronreflectometrydata
AT kiricheko influenceoftheliquidheliummeniscusonneutronreflectometrydata
AT charltontr influenceoftheliquidheliummeniscusonneutronreflectometrydata
AT mcclintockpve influenceoftheliquidheliummeniscusonneutronreflectometrydata
first_indexed 2025-12-07T21:14:38Z
last_indexed 2025-12-07T21:14:38Z
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