Structures and optical properties of solid hydrogen at ultrahigh pressures

We have studied the electronic energy bands for the structures whose primitive cell contains up to four molecules, with full optimization of the structures, based on the GGA and LDA band calculations. Above 250 GPa, the eventual optimal structure obtained by the GGA or the LDA calculation is Cmca, w...

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Veröffentlicht: Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України 2003
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spelling nasplib_isofts_kiev_ua-123456789-1289122025-02-23T17:22:59Z Structures and optical properties of solid hydrogen at ultrahigh pressures Hitose Nagara High-Pressure Studies We have studied the electronic energy bands for the structures whose primitive cell contains up to four molecules, with full optimization of the structures, based on the GGA and LDA band calculations. Above 250 GPa, the eventual optimal structure obtained by the GGA or the LDA calculation is Cmca, which is a layered structure with the molecular bonds lying in planes, and has a metallic band structure with no band gaps. The metallic property of the band structure still remains unchanged even if the molecular bonds in the plane of the Cmca were inclined such that the atoms in the molecule escape from the plane. The electronic bands of the Cmca and those of some other candidate structures are discussed in the light of recent experimental result. Effects of the occupation of electronic states on the predicted optimal structures are also studied. This work is supported by Grant-in-Aid for COE Research (10CE2004) of the Ministry of Education, Culture, Sports, Science and Technology of Japan. 2003 Article Structures and optical properties of solid hydrogen at ultrahigh pressures / Hitose Nagara // Физика низких температур. — 2003. — Т. 29, № 9-10. — С. 947-950. — Бібліогр.: 12 назв. — англ. 0132-6414 PACS: 62.50.+p, 61.50.Ah, 71.30.+h https://nasplib.isofts.kiev.ua/handle/123456789/128912 en Физика низких температур application/pdf Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
language English
topic High-Pressure Studies
High-Pressure Studies
spellingShingle High-Pressure Studies
High-Pressure Studies
Hitose Nagara
Structures and optical properties of solid hydrogen at ultrahigh pressures
Физика низких температур
description We have studied the electronic energy bands for the structures whose primitive cell contains up to four molecules, with full optimization of the structures, based on the GGA and LDA band calculations. Above 250 GPa, the eventual optimal structure obtained by the GGA or the LDA calculation is Cmca, which is a layered structure with the molecular bonds lying in planes, and has a metallic band structure with no band gaps. The metallic property of the band structure still remains unchanged even if the molecular bonds in the plane of the Cmca were inclined such that the atoms in the molecule escape from the plane. The electronic bands of the Cmca and those of some other candidate structures are discussed in the light of recent experimental result. Effects of the occupation of electronic states on the predicted optimal structures are also studied.
format Article
author Hitose Nagara
author_facet Hitose Nagara
author_sort Hitose Nagara
title Structures and optical properties of solid hydrogen at ultrahigh pressures
title_short Structures and optical properties of solid hydrogen at ultrahigh pressures
title_full Structures and optical properties of solid hydrogen at ultrahigh pressures
title_fullStr Structures and optical properties of solid hydrogen at ultrahigh pressures
title_full_unstemmed Structures and optical properties of solid hydrogen at ultrahigh pressures
title_sort structures and optical properties of solid hydrogen at ultrahigh pressures
publisher Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
publishDate 2003
topic_facet High-Pressure Studies
url https://nasplib.isofts.kiev.ua/handle/123456789/128912
citation_txt Structures and optical properties of solid hydrogen at ultrahigh pressures / Hitose Nagara // Физика низких температур. — 2003. — Т. 29, № 9-10. — С. 947-950. — Бібліогр.: 12 назв. — англ.
series Физика низких температур
work_keys_str_mv AT hitosenagara structuresandopticalpropertiesofsolidhydrogenatultrahighpressures
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fulltext Fizika Nizkikh Temperatur, 2003, v. 29, Nos. 9/10, p. 947–950 Structures and optical properties of solid hydrogen at ultrahigh pressures Hitose Nagara Division of Materials Physics, Graduate School of Engineering Science, Osaka University Toyonaka, Osaka 560-8531, Japan E-mail: nagara@mp.es.osaka-u.ac.jp We have studied the electronic energy bands for the structures whose primitive cell contains up to four molecules, with full optimization of the structures, based on the GGA and LDA band cal- culations. Above 250 GPa, the eventual optimal structure obtained by the GGA or the LDA calcu- lation is Cmca, which is a layered structure with the molecular bonds lying in planes, and has a metallic band structure with no band gaps. The metallic property of the band structure still re- mains unchanged even if the molecular bonds in the plane of the Cmca were inclined such that the atoms in the molecule escape from the plane. The electronic bands of the Cmca and those of some other candidate structures are discussed in the light of recent experimental result. Effects of the occupation of electronic states on the predicted optimal structures are also studied. PACS: 62.50.+p, 61.50.Ah, 71.30.+h 1. Introduction Recent experimental study of the compressed hy- drogen revealed nonmetallic behavior at pressures higher than � 300 GPa [1,2]. They report a possibility of the metallization by the closure of the direct elec- tronic band gaps at even higher pressures. The result contradicts many theoretical studies based on the first principles band calculations which predict the closure of indirect band gaps at lower pressures in energeti- cally favorable structures [3–5], and caused a ques- tion about an ability of the band calculations to pre- dict the structures of compressed hydrogen. In spite of the well-known shortcoming of the band calculation based on the local density approximation (LDA) or its modification with the gradient correc- tion (GGA), that is, underestimation of the electronic band gaps, recent first principles band calculations have achieved much success in predicting structures and properties of solids at ambient as well as at high pressures. In the study of compressed hydrogen, whether this shortcoming might hamper the prediction of the structures and mislead us into false structures or not is still unclear because of lacking available experi- mental data of the structure above 100 GPa. In order to check this point at some levels, we have carried out some preliminary calculations and re-ex- amined the structures which have been predicted to be most probable at high pressures, paying attention to the occupation of the electronic bands by the elec- trons. We perform full optimization of the structures above 250 GPa in the GGA and the LDA and study the changes of the electronic bands for structures which appear in the course of the optimization. We compare the results with new type of the calculation [6] which is expected to overcome the shortcoming and discuss the band structures in the light of very re- cent optical measurements [1]. 2. New restrictions imposed on the structures The results of the optical experiment [1] impose new restrictions on the structures from 150 GPa to at least 320 GPa. The first important point to be men- tioned is that the softening of the vibron frequency seems to occur continuously with increasing pressure. No jump of the frequency nor the change of the slope have been observed, which means no drastic changes of the structure. If the structure changes at all, it should be accompanied by a very small change of the vibron frequency. The second point is that the experi- ment reports the features characteristic of a direct band gap, which means the top of the valence band and the bottom of the conduction band are located at the same place in the Brillouin zone. © Hitose Nagara, 2003 In earlier experiments, the vibron frequencies and the optical properties at pressures over 250 GPa were reported and the pressure of direct-gap closure has also been estimated from the optical data [7,8]. The recent optical measurements show the pressures and the character of the optical absorption more clearly. These new results impose important restrictions on the structures of solid hydrogen above the well-known 150 GPa transition. Bearing these points in mind, we examine again some of the structures which have been theoretically studied so far. 3. Calculations and results The structures which can be transformed continu- ously among them are Pca21, Cmc21, Cmca, and Pbca family, which are shown in Fig. 1. Starting from one of those structures, the others are obtained by chang- ing the molecular centers and the molecular orienta- tion continuously. At pressures lower than 200 GPa, the candidates of the most probable structure are Cmc21, Pca21 with hcp molecular centers or its slight modifications [3,4]. The structure, however, becomes unstable at pressures higher than about 200 GPa according to theoretical calculations [3–5]. In those calculations, they used the methods based on the LDA or the GGA which has a shortcoming of underestimating band gaps, resulting in the closure of indirect band gaps at around 200 GPa. Optimization of the structure is a delicate problem and the shortcoming might mislead us into the false optimal structures because of the false occu- pation of the states by the electrons whose energy is in the vicinity of the Fermi level. To investigate the effect of the electron occupation, we performed the calculations restricting the electron occupation. We carried out band calculations using the plane-wave basis functions with energy cut-off of 40 hartree and a pseudo-potential for the ionic potential. Throughout our calculations, we used the packaged codes ABINIT [9] and PHI98PP [10]. 3.1. Preliminary calculations under restricted and unrestricted electronic occupation To study the effect of the false occupation on the optimal structures, we performed following prelimi- nary calculations. First we show an example in which the restricted electron occupation and the unrestricted one give different conclusions in the comparison of to- tal energies. We compare the energies of the Cmc21 and the Pca21 structures with molecular centers fixed at the hcp sites and with c/a fixed at the ideal hcp value (see Fig. 1). We used the unit cell containing 4 mole- cules for both structures. In the first calculation, we performed the usual calculations in which the elec- trons occupy the states with energies lower than the Fermi energy. And in the second one, we restricted the occupation of the electronic states to the lowest 4 branches at each k-point, which simulates the insula- tor type of the electronic occupation of the bands. Up to rs = 1.25, which corresponds to a pressure around 430 GPa, the lowest 4 branches of the electronic en- ergy states in the Cmc21 and the Pca21 seem to be well separated from the 5th branch. Here the rs is the den- sity parameter which is defined by the radius of the sphere, in units of Bohr radius, whose volume is equal to the volume per electron. Comparing the energies of these two structure, we find that the Cmc21 is of lower energy than the Pca21 in the case of the first calculation. On the other hand, in the case of the second calculation, the Pca21 be- comes lower. 3.2. Full optimization of the structures Above example shows the possibility that the false occupation of the electronic states might affect the op- timal structures at each pressure. The change of the occupation occurs when the indirect band gaps disap- pear. Starting from some arrangements of the atomic positions, we then performed full optimization of the structures. As a starting arrangement, we take the Pca21 struc- ture with orthorhombic unit cell containing 4 mole- cules. We have set the molecular centers at ideal hcp lattice sites and at several points between that of the ideal hcp site and the molecular center of the Pbca 948 Fizika Nizkikh Temperatur, 2003, v. 29, Nos. 9/10 Hitose Nagara Pca21 Pbca Cmc21 Cmca � Fig. 1. The structures Pca21, Cmc21, Pbca, and Cmca. Arrows show the directions of molecular axes whose direc- tion consigns with the z axes are positive. These structure can be mutually transformed by continuously changing the molecular centers and orientations. structure (see Fig. 1). The optimization has been done at constant volumes, at rs = 1.40, 1.35, 1.30, and 1.25, which correspond to the pressures around 200, 270, 330, and 430 GPa, respectively. The pressures are esti- mated from the volume dependence of the total energy obtained in our calculations. The LDA calculations show smoother convergence than the GGA ones which contain the calculation of the density gradient. In the optimization of the structures, some runs did not con- verge to any meaningful structures. This is probably due to some problems in the optimization codes. All structures converged and obtained as optimal ones in our runs are of Cmca for rs � 1.35. We note here that the compression seems to be nearly isotropic above 200 GPa (rs � 1.40). Although the molecular centers move from the ideal hcp sites to that of the Cmca, the orthorhombic unit cell is compressed isotropically. At highest density rs = 1.25, the c/a of the orthorhombic lattice decreased about 3 % and the b/a (distance between the layers) increased about 3 %, with molecular bonds tilted about 76� from the z axes and the bond length 1.41a0. They did not show any molecular dissociation at all densities studied. These results are same as those obtained from the usual calculations with no restriction of the band oc- cupation for both GGA and the LDA. 4. Changes of the electronic band structure We study then the changes in the electronic band structures for those structures studied in the optimiza- tion process. The Cmc21 structure is also a layered structure with molecular bonds lying in the planes. The Cmc21 space group holds for any position of the molecular center between the hcp site and the molecu- lar center of the Cmca. When the molecular bond is inclined in a certain way in the Cmc21 and two atoms of the molecule are off the plane, the structure be- comes Pca21. For the extreme case of the Pca21 in which the molecular center is moved to that of the Cmca, the space group becomes Pbca. To compare the band structures we take the nonprimitive unit cell containing 4 molecules for all structures studied. All structures, except for the Cmca, have the band structure in which the lowest 4 branches are well separated from higher ones up to the highest densities rs = 1.25. The indirect band gaps, however, closes at much lower densities. The gaps be- comes wider when the molecules in the Cmc21 are tilted toward the Pca21 structure. The Cmca has the band structure completely differ- ent from the others, where the band structure has no band gaps. The lowest 4 branch touches the higher ones at some points on the �-, �- and c-lines. The na- ture of the touching is line-type [3]. We show in Fig. 2 the band structure of the Cmca taking the nonprimitive unit cell. Even when the molecular bonds are tilted towards the Pbca structure, the me- tallic band character still remains unchanged, though the changes of the distances between the branches are observed at several points in the Brillouin zone. In Fig. 2, we compare the band structure of the Cmca with that of the Pbca at rs = 1.25. It should be noted that the touching of the branches are due to the symmetry properties of the structure, independent of the approximation GGA or LDA used in the calculations. The distance among the branches depends on the approximation. 5. Discussion and summary We discuss these results in the light of the recent optical measurements. Although the Cmca is energeti- cally most favorable, it may be excluded because of the metallic character of band structure. The large fluctuation of the molecular orientation remaining in the Cmca structure [11] might change the electronic Structures and optical properties of solid hydrogen at ultrahigh pressures Fizika Nizkikh Temperatur, 2003, v. 29, Nos. 9/10 949 E n e rg y , e V 30 25 20 15 10 5 0 –5 –10 –15 –20 Y X ��� a E n e rg y , e V 30 25 20 15 10 5 0 –5 –10 –15 –20 Y X ��� b Fig. 2. The electronic band structures for the Cmca (a) and the Pbca (b) at rs = 1.25. To compare the changes in the energy bands, we used the nonprimitive unit cell con- taining 4 molecules for the Cmca structure whose primi- tive cell contains 2 molecules. bands. The metallic character of the electronic bands of the Pbca, however, may offer some negative insight into the changes of the band structure due to the fluc- tuation, although the movement from the Cmca to the Pbca is coherent. The possible fluctuation of the mo- lecular center leaving the positions of the Cmca to- ward those of the Cmc21, however, might lift the me- tallic character of the electronic bands. If the energetically favorable Cmca structure is denied, there will remain two possibilities. One is that there are some other structures which we have overlooked in our study. An example is a structure of larger unit cell [4]. The second possibility is the case that all of the present GGA and LDA based calculations fail to pre- dict energetically favorable structures of compressed hydrogen. In that case, the structure might remain those which is close to the Cmc21 or Pca21 up to at least 320 GPa. The possibility of the second case has been reported recently in the new type of calculation [6] which is designed to overcome the shortcoming of the GGA and the LDA, though the optimization of the structures has not been carried out by that type of cal- culations owing mainly to machine resources. We mention here the low lying librational and phonon modes observed in Raman experiments [12]. The Pca21 has 9 optical phonons and 8 librational modes which are Raman active, and the Cmc21 has 3 optical phonons and 4 librational such modes, while the Cmca has only 4 librational modes with no Raman active optical phonons. Finally we mention that the metallization, which is predicted to occur at � 450 GPa by the extrapolation of the absorption edge to higher pressure, might hap- pen at some lower pressures when the metallization is due to the closure of the indirect band gaps [8]. We have studied the optimal structures and the electronic bands in those energetically favorable struc- tures. The new results of the optical measurements brought about new problems into the theoretical stud- ies of compressed hydrogen. Acknowledgments This work is supported by Grant-in-Aid for COE Research (10CE2004) of the Ministry of Education, Culture, Sports, Science and Technology of Japan. 1. P. Loubeyre, F. Occelli, and R. LeToullec, Nature 416, 613 (2002). 2. C. Narayana, H. Luo, J. Orloff, and A.L. Ruoff, Nature 393, 46 (1998). 3. K. Nagao, T. Takezawa, and H. Nagara, Phys. Rev. B59, 13741 (1999). 4. J. Kohanoff, S. Scandolo, S. Gironcoli, and E. To- satti, Phys. Rev. Lett. 83, 4097 (1999). 5. K.A. Jonson and N.W. Ashkroft, Nature 403, 632 (2000). 6. M. Stadele and R.M. Martin, Phys. Rev. Lett. 84, 6070 (2000). 7. H.K. Mao and R.J. Hemly, Science 244, 1462 (1989). 8. M. Hanfland, R.J. Hemly, and H.K. Mao, Phys. Rev. B43, 8767 (1991). 9. The ABINIT code is a common project of the Université Catholique de Louvain, Corning Incorporated, and other contributors, URL http://www.abinit.org. 10. M. Fuchs and M. Scheffler, Comput. Phys. Commun. 119, 67 (1999), URL http:// www.fhi-berlin.mpg.de/th/fhi98vd/fhi98PP/index. html. 11. H. Kitamura, S. Tsuneyuki, T. Ogitsu, and T. Miyake, Nature 404, 259 (2000). 12. A.F. Goncharov, R.J. Hemly, H.K. Mao, and J. Shu, Phys. Rev. Lett. 80, 101 (1998). 950 Fizika Nizkikh Temperatur, 2003, v. 29, Nos. 9/10 Hitose Nagara