Investigation of magnetic flux gradients in hard superconductors

Analytical calculations of the transverse magnetostriction in a thin hard superconductor are presented in relation to the distributions of currents and fields within a superconducting specimen in a varied magnetic field. The approach is successfully tested on high-temperature superconductors. The fl...

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Published in:Физика низких температур
Date:2001
Main Authors: Bruk, V.V., Eremenko, V.V., Makedonskaya, N.I., Shabakayeva, Yu.A., Sirenko, V.A.
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Language:English
Published: Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України 2001
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Online Access:https://nasplib.isofts.kiev.ua/handle/123456789/130021
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Cite this:Investigation of magnetic flux gradients in hard superconductors / V.V. Bruk, V.V. Eremenko, N.I. Makedonskaya, Yu.A. Shabakayeva, V.A. Sirenko // Физика низких температур. — 2001. — Т. 27, № 4. — С. 419-424. — Бібліогр.: 13 назв. — англ.

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author Bruk, V.V.
Eremenko, V.V.
Makedonskaya, N.I.
Shabakayeva, Yu.A.
Sirenko, V.A.
author_facet Bruk, V.V.
Eremenko, V.V.
Makedonskaya, N.I.
Shabakayeva, Yu.A.
Sirenko, V.A.
citation_txt Investigation of magnetic flux gradients in hard superconductors / V.V. Bruk, V.V. Eremenko, N.I. Makedonskaya, Yu.A. Shabakayeva, V.A. Sirenko // Физика низких температур. — 2001. — Т. 27, № 4. — С. 419-424. — Бібліогр.: 13 назв. — англ.
collection DSpace DC
container_title Физика низких температур
description Analytical calculations of the transverse magnetostriction in a thin hard superconductor are presented in relation to the distributions of currents and fields within a superconducting specimen in a varied magnetic field. The approach is successfully tested on high-temperature superconductors. The flux distribution derived from magnetostriction measurements is in satisfactory agreement with that obtained from computer processing of magnetooptical images. The magnetic flux distribution below the irreversibility line of hard superconductors is derived from both original magnetization and magnetostriction measurements and image processing. Perfect consistency of the results is obtained for a family of high-temperature superconductors (La₂₋xSrxCuO₄, Bi₂Sr₂CaCu₂Ox, YBa₂Cu₃O₇₋d).
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fulltext Fizika Nizkikh Temperatur, 2001, v. 27, No. 4, p. 419–424 Br uk V. V., E re men ko V. V., Maked onskaya N. I. , Sha baka yeva Yu. A ., an d Sire nko V. A .Investig ation of m ag netic flux g rad ie nts in har d super con duct orsBr uk V. V., E re men ko V. V., Maked onskaya N. I. , Sha baka yeva Yu. A ., an d Sire nko V. A .Investig ation of m ag netic flux g rad ie nts in har d super con duct ors Investigation of magnetic flux gradients in hard superconductors V. V. Bruk, V. V. Eremenko, N. I. Makedonskaya, Yu. A. Shabakayeva, and V. A. Sirenko B. Verkin Institute for Low Temperature Physics and Engineering of the National Academy of Sciences of Ukraine 47 Lenin Ave., Kharkov 61164, Ukraine E-mail: shabakayeva@ilt.kharkov.ua Received October 26, 2000 Analytical calculations of the transverse magnetostriction in a thin hard superconductor are pre- sented in relation to the distributions of currents and fields within a superconducting specimen in a varied magnetic field. The approach is successfully tested on high-temperature superconductors. The flux distribution derived from magnetostriction measurements is in satisfactory agreement with that obtained from computer processing of magnetooptical images. The magnetic flux distribution below the irre- versibility line of hard superconductors is derived from both original magnetization and magnetostriction measurements and image processing. Perfect consistency of the results is obtained for a family of high-temperature superconductors (La2−xSrxCuO4 , Bi2Sr2CaCu2Ox , YBa2Cu3O7−δ). PACS: 75.30.Kz Introduction Measurements of the irreversible «giant» magne- tostriction in HTSC [1–4] appears to be an effective tool for examination of the pinning-related phe- nomena in hard superconductors. The 1D case was considered in detail for a thin long strip in a longitudinal magnetic field [5], and good agreement was achieved with the conventional models [6-9] of the magnetic flux distributions in type-II supercon- ductors. In Ref. 10 another typical experimental situation is analyzed which corresponds to an exter- nal magnetic field normal to the flat face of a thin superconductor. Such a situation is frequently real- ized during magnetization and magnetic flux dis- tribution measurements the thin films and single crystals of HTSC. It is not straightforwardly de- scribed by the classical models and their extensions, and it requires taking the demagnetizing effects into account. The problems of the current and flux distributions in these geometries are widely dis- cussed in the literature (see, e.g., Ref. 11 and the references therein). In this work we present analy- tical estimations of the relevant magnetostrictions and show that their measurements can elucidate some aspects of the problem. Calculations It follows from Refs. 1–4 that the irreversible magnetostriction of HTSC with high critical cur- rent densities jc is caused by the pressure of the magnetic field, which smears the magnetic flux within a specimen with strong pinning. The rele- vant reduced strain of a superconductor in a mag- netic field is related to the magnetic flux distribu- tion inside the sample by the elastic equations taking into account the balance of forces in a system «flux line lattice imperfection», provided that the fully penetrated state has been established [1]: ∆L L = − 1 L ∫ −L/2 L/2 Be 2 − B2(x) µ0E dx , (1) where L is the sample size, Be = µ0He is the mag- netic induction corresponding to the external mag- netic field He , B(x) is the local flux density in the sample, E is the Young’s modulus along the length change and µ0 is the permeability of vacuum. We consider a thin flat sample of thickness d and width 2a under the action of a varied field perpendicular to the face of the sample [10] (Fig. 1). If the specimen is assumed to be infinite in one direction z © V. V. Bruk, V. V. Eremenko, N. I. Makedonskaya, Yu. A. Shabakayeva, and V. A. Sirenko, 2001 and Be to be uniform along the x axis, the flux gradients are in the y direction. In this case the longitudinal component of Be merely corresponds to the shielding currents, while the transverse compo- nent is responsible for the flux profiles, and so it alone determines the magnetostrictive strain, which is consequently directed along y. B(y) is determined by the Maxwell equations. The elastic stresses in the sample are calculated following [10]. Accordingly, the transverse magne- tostriction (1) reads: ∆L L = 1 E ∫ 0 1 σ(η) dη , (2) which is equal to [10] ∆L L = 1 E µ0 jcda π      π 2 (cm − c1)hm + πc1 2 h − − cm Artanh      √k1 2 − km 2 k1      + c1 2 Artanh      √k1 2 − km 2 cmk1           + + 1 E µ0 jcda π F(km , k1) , (3) where σ(η) is elastic stresses in the sample; η ≡ y a ∈ [− 1, 1] ; cm ≡ √1 − km 2 = tanh (πhm ) ; c1 ≡ √1 − k1 2 = tanh (πh1) ; hm ≡ Bm µ0 jcd ; h ≡ Be µ0 jcd ; h1 ≡ Bm − Be 2µ0 jcd ; k1 ≡ cosh−1 (πh1) ; km ≡ cosh−1 m(πhm ) ; F(km , k1) = = 2 π        k1M(km , k1 , x = k1) − ∫ k m k 1 M(km , k1 , x) dx        ; Bm corresponds to the maximum field in a magneti- zation cycle. The calculations of ∆L/L using flux gradients determined from magnetization measurements are presented in Fig. 1. It was anticipated that estimate of the flux gradients from magnetooptical image processing would also be used in these calculations. This is illustrated below on the YBa2Cu3O7−δ samples. The process of determination of magnetic flux distribution from magnetooptical image consists of two stages using the magnetooptical method and the method of computer processing. The principle of visualization of magnetic flux structure in high-Tc superconductors, based on the Faraday effect, is shown in Fig. 2,a. The supercon- ducting sample was covered with a garnet film doped with bismith. The external magnetic field was applied parallel to the c axis of the sample. The magnetic flux profile was determined by observing changes of the domain structure. The domain struc- ture (in a garnet film placed above the supercon- ducting sample) was observed as a function of magnetic field intensity and may be regarded as magnetic flux sensor. The visual pattern of magnetic flux trapping in the YBa2Cu3O7−δ sample when the external mag- netic field is decreased from some maximum value to zero is shown in Fig. 2,b. The magnetooptical image obtained is subjected to preliminary com- puter processing. Applying computer methods for image processing allowed us to examine the trapped magnetic flux distribution both on a qualitive level and to perform quantitative estimations of the local magnetic in- duction (Be) distribution over the sample surface. When a Bi-containing iron garnet film was used as Fig. 1. Simulated magnetostriction loops of the La1.85Sr0.15CuO4 in a transverse magnetic field for different hm : 2.5 (1); 5 (2); 12.5 (3); 25 (4). V. V. Bruk, V. V. Eremenko, N. I. Makedonskaya, Yu. A. Shabakayeva, and V. A. Sirenko 420 Fizika Nizkikh Temperatur, 2001, v. 27, No. 4 indicator, the preliminary stage of computer pro- cessing included low-frequency spatial image filter- ing in order to eliminate the disturbances induced by the labyrinth magnetic structure in the regions of Be below the saturation field. For this reason the initial image was scanned by a sliding window of square shape with a size a few times larger than the period of the labyrinth structure. For each selected window a two-dimensional Fourier transform was performed, the high-frequency harmonics associated with the labyrinth structure were filtered out, and inverse Fourier transform was performed. When a film with in-plane anisotropy was used as a indica- tor, there was no need of the preliminary image processing. In order to obtain a quantitative estimate of the local magnetic induction after the low-frequency image filtering a segmentation of the latter was performed by separation of the regions with the comparatively uniform values of beam light inten- sity. This segmentation was based on analysis of a histogram of the numerical equivalents of the image brightness. In the interactive mode the brightness values were shown on the histogram, which corre- sponded to the boundaries between the separated grades of the image elements. To visualize the segmented image, all elements within the separated grade were coded by a definite color. The transition to quantitative estimates was based on the following assumptions: a) the angle between the transmission planes of the polarizer and analyzer did not differ much from the normal one; b) trapped magnetic flux rotates the plane of polarization by small angle. The first assumption means that the intensity of the registered light beam is linear in the second power of the sine of the rotation angle ϕ of the plane of polarization: I = I0 sin 2 ϕ. The second as- sumption allows the sine of the small angle to be replaced by the angle itself expressed in radians: I ≈ I0ϕ2. Taking into account that ϕ ∼ B, one ob- tains I ∼ α2B2, where α is a linear factor deter- mined by the sample surface, B is the integral value of the magnetic induction. A pattern of the obtained distribution of the local magnetic induction is shown in Fig. 3. In addition the computer processing allows one to analyze the surface distribution of the local values of the Be and Be 2 gradients, the latter being directly connected with the pinning force. In order to study the spatial distribution of the Be 2 gradient the image was spatially differentiated using the Sobel operator [12]. For this reason the projections of the image brightness gradients were calculated (in arbitrary integer units) along the axes x and y by the method of image convolution with masks of the Sobel operator: Hx =      −1, 0, 1 −2, 0, 2 −1, 0, 1      ; Hy =      1, 2, 1 0, 0, 0 −1, −2, −1      , ∂I ∂x(y) (jx , jy) = = ∑ i x =−1 1 ∑ i y =−1 1 I(jx + ix , jy + iy)Hx(y)(ix + 2, iy + 2) , (4) Fig. 2. Magnetooptical scheme: a) 1 — HTSC, 2 — indicator; −k, +k — transmitted and reflected light, respectively, Be — external magnetic field; b) visualization of trapping of magnetic flux in the sample of YBa2Cu3O7−δ (T = 14 K). a b Investigation of magnetic flux gradients in hard superconductors Fizika Nizkikh Temperatur, 2001, v. 27, No. 4 421 where jx , jy are the numbers of the row and co- lumn, respectively, with the intersection corre- sponding to the image element for which the gra- dient value is estimated. Further, the modulus of the gradient is calcu- lated according to the equation:    ∂Be 2 ∂ r    = α 12b       ∂I ∂x    2 +    ∂I ∂y    2    1/2 , (5) where b is the size of a single pixel of the image. The appearance of the factor α/12b may be explained by the following equation: ∂B ∂x = α 3    I13 − I31 2 √2 b 1 √2 + I23 − I12 2b + I33 − I11 2 √2b 1 √2    = = α 12b [2(I23 − I12) + (I13 − I31) + (I33 − I11)] , (6) where Ii,j is the intensity for the image element with the row number i and column number j in the selected window (i, j = 1–3). A similar formula may be written for ∂B/∂y also. Then    ∂B ∂ r    =       ∂B ∂x    2 +    ∂B ∂y    2    1/2 . In Fig. 4 a typical distribution of pinning force is presented. It is seen from the figure that the maximum values of |∂Be 2/∂r| are observed within the boundary of the trapped magnetic flux region. Estimaties of the |∂Be/∂r| values were made in order to study the dependence of this characteristic on Be and hence to estimate magnetostriction with respect to (3). The calculations were performed along different lines within the image, on going from the boun- daries of the trapped magnetic flux region to the region of maximum values of I using the following equations:    ∂Be ∂r    = 1 2Be    ∂Be 2 ∂r    , (7) Be = α √I . (8) For qualitative analysis of the obtained depend- ence the dispersion diagrams were constructed in the plane Be − |∂Be/∂r|. A typical scatter diagram is presented in Fig. 5. As is seen from the figure the gradient initially increases with Be and then de- creases. Fig. 3. Distribution of local magnetic induction, mT (filtered pattern). Fig. 4. Distribution of pinning force Fp , N/mm2 for a frag- ment outlined in Fig. 3. V. V. Bruk, V. V. Eremenko, N. I. Makedonskaya, Yu. A. Shabakayeva, and V. A. Sirenko 422 Fizika Nizkikh Temperatur, 2001, v. 27, No. 4 Experimental data The magnetostriction and magnetization meas- urements were performed on a single crystal of YBa2Cu3O7−δ . The superconducting transition temperature was determined from the temperature dependence of zero-field-cooled magnetization and equalled TSN = 92 K. The magnetostriction was measured by strain gauges along different crystal- lographic directions with an external magnetic field perpendicular to the face of the sample. The magne- tization of the sample was measured in a vibrational magnetometer. The experimental geometry used al- lowed us to control the surface flux distributions with magnetooptical sensors by utilizing demagne- tizing effects. Figure 6 shows the magnetostriction of YBa2Cu3O7−δ at 14 K. A more detailed analysis of the magneto- striction gives good agreement between the theory and experiment. We have obtained the width of the magnetostriction hysteresis loop at 14 K in a mag- netic field of 12 T about 2⋅10−5 both theoretically, using formula (3), and experimentally. The Young’s moduli of YBa2Cu3O7−δ along the direction of the magnetostriction measurements were calculated from the following equation: 1 E = c22c33 − c23 2 c11c22c33 + 2c12c13c23 − c11c23 2 − c22c13 2 − c33c12 2 + + ny 2[c33(c11 − c22) + c13 2 − c23 2 ] + nz 2[c22(c11 − c33) + c12 2 − c23 2 ] c11c22c33 + 2c12c13c23 − c11c23 2 − c22c13 2 − c33c12 2 + + nx 2ny 2   1 c66 + 2(c13c23 − c12c33) − (c22c33 − c23 2 ) − (c11c33 − c13 2 ) c11c22c33 + 2c12c13c23 − c11c23 2 − c22c13 2 − c33c12 2    + + nx 2nz 2   1 c44 + 2(c12c23 − c22c13) − (c11c22 − c12 2 ) − (c22c33 − c23 2 ) c11c22c33 + 2c12c13c23 − c11c23 2 − c22c13 2 − c33c12 2    + Fig. 6. Experimental and simulated magnetostriction loops for a YBa2Cu3O7−δ single crystal. Fig. 5. Typical scattering diagram Be − |∂Be/∂r|. Investigation of magnetic flux gradients in hard superconductors Fizika Nizkikh Temperatur, 2001, v. 27, No. 4 423 + ny 2nz 2   1 c55 + 2(c12c13 − c11c23) − (c11c33 − c13 2 ) − (c11c22 − c12 2 ) c11c22c33 + 2c12c13c23 − c11c23 2 − c22c13 2 − c33c12 2    (9) where the elastic moduli cik are derived from the acoustic measurements [13], and n is the unit vector along a direction of magnetostriction measurement in the coordinates related to the principle lattice axes. Conclusion A model description of magnetostriction is pro- posed for a thin superconductor in a magnetic field perpendicular to a flat face of the sample. The simulated magnetostriction loop calculated using flux gradients derived from magnetooptical image processing is in a semi-quantitative agreement with the transverse magnetostriction measurements on the single crystal YBa2Cu3O7−δ . The authors acknowledge Dr. S. B. Feodosyev for his assistance in computations. We are grateful to Prof. H. Szymczak for stimulating discussions. 1. H. Ikuta, N. Hirota, Y. Nakayama, K. Kishio, and K. Ki- tazawa, Phys. Rev. Lett. 70, 2166 (1993). 2. C. de la Fuente, A. del Moral, J. I. Arnaudas, and J. S. Abell, Physica C244, 214 (1995). 3. L. Heil, H. Ikuta, K. Kishio, and K. Kitazawa, Physica C235–240, 2925 (1993). 4. A. Schmidt, F. Stellmach, and S. Ewert, Physica B194– 196, 1787 (1994). 5. H. Ikuta, K. Kishio, and K. Kitazawa, J. Appl. Phys. 76, 4776 (1994). 6. C. P. Bean, Phys. Rev. Lett. 8, 250 (1962); Rev. Mod. Phys. 36, 31 (1964). 7. Y. R. Kim, C. F. Hempstead, and A. R. Strnat, Phys. Rev. Lett. 9, 306 (1962); 12, 528 (1963). 8. V. R. Karasik, N. G. Vasil’ev, and V. G. Ershov, Zh. Eksp. Teor. Fiz. 59, 790 (1970) [Sov. Phys. JETP 32, 433 (1971)]. 9. S. Senoussi, J. Phys. III (Paris) 2, 1041 (1992). 10. V. V. Eremenko, V. A. Sirenko, H. Szymczak, and A. Nabialek, Superlattices and Microstructures 24, 221 (1998). 11. E. H. Brandt, Phys. Rev. B54, 4246 (1996). 12. W. K. Pratt, Digital Image Processing, New York, Wiley- Interscience (1978). 13. H. Ledbetter and M. Lei, J. Mater. Res. 6, 2253 (1991). V. V. Bruk, V. V. Eremenko, N. I. Makedonskaya, Yu. A. Shabakayeva, and V. A. Sirenko 424 Fizika Nizkikh Temperatur, 2001, v. 27, No. 4
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institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
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language English
last_indexed 2025-12-07T17:58:53Z
publishDate 2001
publisher Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
record_format dspace
spelling Bruk, V.V.
Eremenko, V.V.
Makedonskaya, N.I.
Shabakayeva, Yu.A.
Sirenko, V.A.
2018-02-04T16:50:06Z
2018-02-04T16:50:06Z
2001
Investigation of magnetic flux gradients in hard superconductors / V.V. Bruk, V.V. Eremenko, N.I. Makedonskaya, Yu.A. Shabakayeva, V.A. Sirenko // Физика низких температур. — 2001. — Т. 27, № 4. — С. 419-424. — Бібліогр.: 13 назв. — англ.
0132-6414
PACS: 75.30.Kz
https://nasplib.isofts.kiev.ua/handle/123456789/130021
Analytical calculations of the transverse magnetostriction in a thin hard superconductor are presented in relation to the distributions of currents and fields within a superconducting specimen in a varied magnetic field. The approach is successfully tested on high-temperature superconductors. The flux distribution derived from magnetostriction measurements is in satisfactory agreement with that obtained from computer processing of magnetooptical images. The magnetic flux distribution below the irreversibility line of hard superconductors is derived from both original magnetization and magnetostriction measurements and image processing. Perfect consistency of the results is obtained for a family of high-temperature superconductors (La₂₋xSrxCuO₄, Bi₂Sr₂CaCu₂Ox, YBa₂Cu₃O₇₋d).
The authors acknowledge Dr. S. B. Feodosyev
 for his assistance in computations. We are grateful
 to Prof. H. Szymczak for stimulating discussions.
en
Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України
Физика низких температур
Низкотемпеpатуpная магнитостpикция магнетиков и свеpхпpоводников
Investigation of magnetic flux gradients in hard superconductors
Article
published earlier
spellingShingle Investigation of magnetic flux gradients in hard superconductors
Bruk, V.V.
Eremenko, V.V.
Makedonskaya, N.I.
Shabakayeva, Yu.A.
Sirenko, V.A.
Низкотемпеpатуpная магнитостpикция магнетиков и свеpхпpоводников
title Investigation of magnetic flux gradients in hard superconductors
title_full Investigation of magnetic flux gradients in hard superconductors
title_fullStr Investigation of magnetic flux gradients in hard superconductors
title_full_unstemmed Investigation of magnetic flux gradients in hard superconductors
title_short Investigation of magnetic flux gradients in hard superconductors
title_sort investigation of magnetic flux gradients in hard superconductors
topic Низкотемпеpатуpная магнитостpикция магнетиков и свеpхпpоводников
topic_facet Низкотемпеpатуpная магнитостpикция магнетиков и свеpхпpоводников
url https://nasplib.isofts.kiev.ua/handle/123456789/130021
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AT shabakayevayua investigationofmagneticfluxgradientsinhardsuperconductors
AT sirenkova investigationofmagneticfluxgradientsinhardsuperconductors