On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes

Investigation of multiple low-temperature mixed crystallization (LTMC) of the solution wastes of cesium iodide was reported. LTMC is a very simple and convenient way for an essential decrease of the concentrations of practically all the admixtures including isomorphic ones (Na, K, Rb). However, LTMC...

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Опубліковано в: :Functional Materials
Дата:2017
Автори: Boyarintsev, A.Yu., Cherginets, V.L., Ponomarenko, T.V., Rebrova, T.P., Varich, A.G., Bryleva, E.Yu., Koryakina, E.M., Sheina, T.V., Varchenko, V.V., Yurchenko, O.I.
Формат: Стаття
Мова:English
Опубліковано: НТК «Інститут монокристалів» НАН України 2017
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Онлайн доступ:https://nasplib.isofts.kiev.ua/handle/123456789/136880
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Назва журналу:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Цитувати:On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes / A.Yu. Boyarintsev, V.L. Cherginets, T.V. Ponomarenko, T.P. Rebrova, A.G. Varich, E.Yu. Bryleva, E.M. Koryakina, T.V. Sheina, V.V. Varchenko, O.I. Yurchenko // Functional Materials. — 2017. — Т. 24, № 4. — С. 640-648. — Бібліогр.: 15 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
id nasplib_isofts_kiev_ua-123456789-136880
record_format dspace
spelling Boyarintsev, A.Yu.
Cherginets, V.L.
Ponomarenko, T.V.
Rebrova, T.P.
Varich, A.G.
Bryleva, E.Yu.
Koryakina, E.M.
Sheina, T.V.
Varchenko, V.V.
Yurchenko, O.I.
2018-06-16T17:17:06Z
2018-06-16T17:17:06Z
2017
On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes / A.Yu. Boyarintsev, V.L. Cherginets, T.V. Ponomarenko, T.P. Rebrova, A.G. Varich, E.Yu. Bryleva, E.M. Koryakina, T.V. Sheina, V.V. Varchenko, O.I. Yurchenko // Functional Materials. — 2017. — Т. 24, № 4. — С. 640-648. — Бібліогр.: 15 назв. — англ.
1027-5495
DOI: https://doi.org/10.15407/fm24.04.640
https://nasplib.isofts.kiev.ua/handle/123456789/136880
Investigation of multiple low-temperature mixed crystallization (LTMC) of the solution wastes of cesium iodide was reported. LTMC is a very simple and convenient way for an essential decrease of the concentrations of practically all the admixtures including isomorphic ones (Na, K, Rb). However, LTMC results in CsI enriching with Tl, which enters into the crystallized fraction. Due to the presence of considerable amounts of Na and sulfate admixtures during the first 3-4 LTMC the displacement of other admixtures occurs with lower intensity comparing with the following LTMC stages and the threshold concentration of Na is ca. 5·10⁻² mas.%. For Na the effective purification coefficient β is 0.6-0.7 for the initial solution and it reduces to 0.35-0.5 in more pure solutions, for K these values are 0.75 and 0.5-0.55. Na content does not affect Rb distribution and for this admixture β ~ 0.65-0.75 for all the solutions. For Cu the value of β is close to 1 since CuI is insoluble in water and LTMC favors its entering in the solid fraction. β value for Tl admixture is ca. 1.06 that means the enriching of the final product of LTMC with respect to this admixture. The removal of sulfates from CsI using LTMC occurs very easy.
en
НТК «Інститут монокристалів» НАН України
Functional Materials
Technology
On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes
Article
published earlier
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
title On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes
spellingShingle On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes
Boyarintsev, A.Yu.
Cherginets, V.L.
Ponomarenko, T.V.
Rebrova, T.P.
Varich, A.G.
Bryleva, E.Yu.
Koryakina, E.M.
Sheina, T.V.
Varchenko, V.V.
Yurchenko, O.I.
Technology
title_short On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes
title_full On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes
title_fullStr On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes
title_full_unstemmed On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes
title_sort on some features of low-temperature mixed crystallization of csi solutions obtained from industrial wastes
author Boyarintsev, A.Yu.
Cherginets, V.L.
Ponomarenko, T.V.
Rebrova, T.P.
Varich, A.G.
Bryleva, E.Yu.
Koryakina, E.M.
Sheina, T.V.
Varchenko, V.V.
Yurchenko, O.I.
author_facet Boyarintsev, A.Yu.
Cherginets, V.L.
Ponomarenko, T.V.
Rebrova, T.P.
Varich, A.G.
Bryleva, E.Yu.
Koryakina, E.M.
Sheina, T.V.
Varchenko, V.V.
Yurchenko, O.I.
topic Technology
topic_facet Technology
publishDate 2017
language English
container_title Functional Materials
publisher НТК «Інститут монокристалів» НАН України
format Article
description Investigation of multiple low-temperature mixed crystallization (LTMC) of the solution wastes of cesium iodide was reported. LTMC is a very simple and convenient way for an essential decrease of the concentrations of practically all the admixtures including isomorphic ones (Na, K, Rb). However, LTMC results in CsI enriching with Tl, which enters into the crystallized fraction. Due to the presence of considerable amounts of Na and sulfate admixtures during the first 3-4 LTMC the displacement of other admixtures occurs with lower intensity comparing with the following LTMC stages and the threshold concentration of Na is ca. 5·10⁻² mas.%. For Na the effective purification coefficient β is 0.6-0.7 for the initial solution and it reduces to 0.35-0.5 in more pure solutions, for K these values are 0.75 and 0.5-0.55. Na content does not affect Rb distribution and for this admixture β ~ 0.65-0.75 for all the solutions. For Cu the value of β is close to 1 since CuI is insoluble in water and LTMC favors its entering in the solid fraction. β value for Tl admixture is ca. 1.06 that means the enriching of the final product of LTMC with respect to this admixture. The removal of sulfates from CsI using LTMC occurs very easy.
issn 1027-5495
url https://nasplib.isofts.kiev.ua/handle/123456789/136880
citation_txt On some features of low-temperature mixed crystallization of CsI solutions obtained from industrial wastes / A.Yu. Boyarintsev, V.L. Cherginets, T.V. Ponomarenko, T.P. Rebrova, A.G. Varich, E.Yu. Bryleva, E.M. Koryakina, T.V. Sheina, V.V. Varchenko, O.I. Yurchenko // Functional Materials. — 2017. — Т. 24, № 4. — С. 640-648. — Бібліогр.: 15 назв. — англ.
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