Thermomagnetic studies of thermoexfoliated graphite-transition metal composites

Thermal stability and magnetic susceptibility of thermoexfoliated graphite-metal (TEG-Me) composites have been investigated in the temperature range 300-850 K. The TEG-Me (Co, Ni) composites have been produced by the metal cation reduction in aqueous medium with sodium tetrahydroborate. The structur...

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Published in:Functional Materials
Date:2007
Main Authors: Vovchenko, L.L., Babich, M.G., Zakharenko, M.I., Brusilovets, A.I., Kapitanchuk, L.M.
Format: Article
Language:English
Published: НТК «Інститут монокристалів» НАН України 2007
Online Access:https://nasplib.isofts.kiev.ua/handle/123456789/136988
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Journal Title:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Cite this:Thermomagnetic studies of thermoexfoliated graphite-transition metal composites / L.L. Vovchenko, M.G. Babich, M.I. Zakharenko, A.I. Brusilovets, L.M. Kapitanchuk // Functional Materials. — 2007. — Т. 14, № 3. — С. 378-381. — Бібліогр.: 7 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
id nasplib_isofts_kiev_ua-123456789-136988
record_format dspace
spelling Vovchenko, L.L.
Babich, M.G.
Zakharenko, M.I.
Brusilovets, A.I.
Kapitanchuk, L.M.
2018-06-16T18:24:43Z
2018-06-16T18:24:43Z
2007
Thermomagnetic studies of thermoexfoliated graphite-transition metal composites / L.L. Vovchenko, M.G. Babich, M.I. Zakharenko, A.I. Brusilovets, L.M. Kapitanchuk // Functional Materials. — 2007. — Т. 14, № 3. — С. 378-381. — Бібліогр.: 7 назв. — англ.
1027-5495
https://nasplib.isofts.kiev.ua/handle/123456789/136988
Thermal stability and magnetic susceptibility of thermoexfoliated graphite-metal (TEG-Me) composites have been investigated in the temperature range 300-850 K. The TEG-Me (Co, Ni) composites have been produced by the metal cation reduction in aqueous medium with sodium tetrahydroborate. The structure and phase composition of the products was characterized using X-ray diffraction, scanning electron microscopy, Auger electron spectroscopy and secondary ion mass spectrometry. The results of these investigations show that the metal in the green composites must exist in the bound state as Me—B and Me—H. The gradual heating (up to 850 K) or annealing (at 825 K) of the TEG-Me composites results in the appearance of ferromagnetic properties. Thermal cycling of TEG-Me composites results in a decreased magnetic susceptibility due to oxidation of metallic particles.
en
НТК «Інститут монокристалів» НАН України
Functional Materials
Thermomagnetic studies of thermoexfoliated graphite-transition metal composites
Термомагнітні дослідження композитів терморозширення графіт-перехідний метал
Article
published earlier
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
title Thermomagnetic studies of thermoexfoliated graphite-transition metal composites
spellingShingle Thermomagnetic studies of thermoexfoliated graphite-transition metal composites
Vovchenko, L.L.
Babich, M.G.
Zakharenko, M.I.
Brusilovets, A.I.
Kapitanchuk, L.M.
title_short Thermomagnetic studies of thermoexfoliated graphite-transition metal composites
title_full Thermomagnetic studies of thermoexfoliated graphite-transition metal composites
title_fullStr Thermomagnetic studies of thermoexfoliated graphite-transition metal composites
title_full_unstemmed Thermomagnetic studies of thermoexfoliated graphite-transition metal composites
title_sort thermomagnetic studies of thermoexfoliated graphite-transition metal composites
author Vovchenko, L.L.
Babich, M.G.
Zakharenko, M.I.
Brusilovets, A.I.
Kapitanchuk, L.M.
author_facet Vovchenko, L.L.
Babich, M.G.
Zakharenko, M.I.
Brusilovets, A.I.
Kapitanchuk, L.M.
publishDate 2007
language English
container_title Functional Materials
publisher НТК «Інститут монокристалів» НАН України
format Article
title_alt Термомагнітні дослідження композитів терморозширення графіт-перехідний метал
description Thermal stability and magnetic susceptibility of thermoexfoliated graphite-metal (TEG-Me) composites have been investigated in the temperature range 300-850 K. The TEG-Me (Co, Ni) composites have been produced by the metal cation reduction in aqueous medium with sodium tetrahydroborate. The structure and phase composition of the products was characterized using X-ray diffraction, scanning electron microscopy, Auger electron spectroscopy and secondary ion mass spectrometry. The results of these investigations show that the metal in the green composites must exist in the bound state as Me—B and Me—H. The gradual heating (up to 850 K) or annealing (at 825 K) of the TEG-Me composites results in the appearance of ferromagnetic properties. Thermal cycling of TEG-Me composites results in a decreased magnetic susceptibility due to oxidation of metallic particles.
issn 1027-5495
url https://nasplib.isofts.kiev.ua/handle/123456789/136988
citation_txt Thermomagnetic studies of thermoexfoliated graphite-transition metal composites / L.L. Vovchenko, M.G. Babich, M.I. Zakharenko, A.I. Brusilovets, L.M. Kapitanchuk // Functional Materials. — 2007. — Т. 14, № 3. — С. 378-381. — Бібліогр.: 7 назв. — англ.
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