Iodine-assisted solid-state synthesis and characterization of nanocrystalline zirconium diboride nanosheets

• Published in: Сверхтвердые материалы
• Date: 2018
• Main Authors: Liangbiao Wang, Dejian Zhao, Qinglin Cheng, Quanquan Lu, Weiqiao Liu, Keyan Bao, Binglong Zhu, Quanfa Zhou
• Format: Article
• Language: English
• Published: Інститут надтвердих матеріалів ім. В.М. Бакуля НАН України 2018
• Subjects: Получение, структура, свойства
• Online Access: https://nasplib.isofts.kiev.ua/handle/123456789/167102
• Journal Title: Digital Library of Periodicals of National Academy of Sciences of Ukraine
• Cite this: Iodine-assisted solid-state synthesis and characterization of nanocrystalline zirconium diboride nanosheets / Liangbiao Wang, Dejian Zhao, Qinglin Cheng, Quanquan Lu, Weiqiao Liu, Keyan Bao, Binglong Zhu, Quanfa Zhou // Сверхтвердые материалы. — 2018. — № 4. — С. 35-40. — Бібліогр.: 18 назв. — англ.

A solid-state route was developed to prepare zirconium diboride nanosheets with the dimension of about 500 nm and thickness of about 20 nm from zirconium dioxide, iodine and sodium borohydride at 700 °C in an autoclave reactor. The obtained ZrB₂ product was investigated by X-ray diffraction, scannin...