HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50

Performed studies of plasma-surface interaction include measurements of plasma energy deposited to the material surface and determination of tungsten cracking threshold during repetitive ITER ELM-like plasma exposures in QSPA Kh-50 with plasma pulses of energy density up to 2.5 MJ/m2 and duration of...

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Дата:2010
Автори: Makhlaj, V.A., Garkusha, I.E., Aksenov, N.N., Kulik, N.V., Landman, I.S., Linke, J., Medvedev, A.V., Malykhin, S.V., Chebotarev, V.V., Pugachev, A.T., Tereshin, V.I.
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Мова:Англійська
Опубліковано: Національний науковий центр «Харківський фізико-технічний інститут» НАН України 2010
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Цитувати:HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50 / V.A. Makhlaj, I.E. Garkusha, N.N. Aksenov, N.V. Kulik, I.S. Landman, J. Linke, A.V. Medvedev, S.V. Malykhin, V.V. Chebotarev, A.T. Pugachev, V.I. Tereshin // Вопросы атомной науки и техники. — 2010. — № 6. — С. 57-59. — Бібліогр.: 8 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
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author Makhlaj, V.A.
Garkusha, I.E.
Aksenov, N.N.
Kulik, N.V.
Landman, I.S.
Linke, J.
Medvedev, A.V.
Malykhin, S.V.
Chebotarev, V.V.
Pugachev, A.T.
Tereshin, V.I.
author_facet Makhlaj, V.A.
Garkusha, I.E.
Aksenov, N.N.
Kulik, N.V.
Landman, I.S.
Linke, J.
Medvedev, A.V.
Malykhin, S.V.
Chebotarev, V.V.
Pugachev, A.T.
Tereshin, V.I.
citation_txt HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50 / V.A. Makhlaj, I.E. Garkusha, N.N. Aksenov, N.V. Kulik, I.S. Landman, J. Linke, A.V. Medvedev, S.V. Malykhin, V.V. Chebotarev, A.T. Pugachev, V.I. Tereshin // Вопросы атомной науки и техники. — 2010. — № 6. — С. 57-59. — Бібліогр.: 8 назв. — англ.
collection DSpace DC
description Performed studies of plasma-surface interaction include measurements of plasma energy deposited to the material surface and determination of tungsten cracking threshold during repetitive ITER ELM-like plasma exposures in QSPA Kh-50 with plasma pulses of energy density up to 2.5 MJ/m2 and duration of 0.25 ms. The energy threshold for tungsten cracking development is found to be ~0,3 MJ/m2. The Ductile-to-Brittle Transition Temperature (DBTT) is experimentally estimated for ITER relevant tungsten grade. Major crack network (cells size up to 1.3 mm) forms only in cases of initial target temperatures below DBTT. Intergranular micro-cracks network (size of cells corresponds to the grain size) appears under heat loads after melting threshold.
first_indexed 2025-12-07T17:21:42Z
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fulltext PROBLEMS OF ATOMIC SCIENCE AND TECHNOLOGY. 2010. 6. 57 Series: Plasma Physics (16), p. 57-59. HIGH HEAT FLUX PLASMA TESTING OF ITER DIVERTOR MATERIALS UNDER ELM RELEVANT CONDITIONS IN QSPA Kh-50 V.A. Makhlaj1, I.E. Garkusha1, N.N. Aksenov1, N.V. Kulik1, I.S. Landman2, J. Linke3, A.V. Medvedev1, S.V. Malykhin4, V.V. Chebotarev1, A.T. Pugachev4, V.I. Tereshin1 1Institute of Plasma Physics NSC “Kharkov Institute of Physics and Technology”, Kharkov, Ukraine; 2Karlsruhe Institute of Technology (KIT), IHM, 76344 Karlsruhe, Germany; 3Forschungszentrum Jülich, IEF 2 D-52425 Juelich, Germany; 4Kharkov Polytechnic Institute, NTU, 61002, Kharkov, Ukraine E-mail: makhlay@ipp.kharkov.ua Performed studies of plasma-surface interaction include measurements of plasma energy deposited to the material surface and determination of tungsten cracking threshold during repetitive ITER ELM-like plasma exposures in QSPA Kh-50 with plasma pulses of energy density up to 2.5 MJ/m2 and duration of 0.25 ms. The energy threshold for tungsten cracking development is found to be ~0,3 J/m2. The Ductile-to-Brittle Transition Temperature (DBTT) is experimentally estimated for ITER relevant tungsten grade. Major crack network (cells size up to 1.3 mm) forms only in cases of initial target temperatures below DBTT. Intergranular micro-cracks network (size of cells corresponds to the grain size) appears under heat loads after melting threshold. PACS: 52.40.Hf 1. INTRODUCTION Divertor armor response to the repetitive plasma impacts during the transient events in ITER and DEMO remains to be one of the most important issues that determine the tokamak performance. Erosion of plasma- facing components (PFCs) restricts the divertor lifetime, leads to contamination of the hot plasma by impurities and can produce a substantial amount of the material dust [1]. The present-day experimental investigations of plasma-surface interaction under conditions simulating ITER transient events are aimed at determination of erosion mechanisms of plasma facing materials, dynamics of erosion products, the impurities transport in the plasma, the vapor shield effects and its influence on plasma energy transfer to the material surface [2-8]. This paper presents recent results of ELM-simulation experiments with the quasi-stationary plasma accelerator QSPA Kh-50. The experiments include study of plasma- surface interaction under inclined plasma impact, the cracks analysis and the results of residual stress measurements for tungsten targets with elongated grains, which is ITER reference W grade. 2. EXPERIMENTAL SETUP AND DIAGNOSTICS Experimental simulations of ITER ELMs (Edge Localized Modes) impacts were performed with quasi- steady-state plasma accelerator QSPA Kh-50 that is largest and most powerful device of this kind [2, 5-8]. The main parameters of QSPA Kh-50 hydrogen plasma streams were as follows: ion impact energy about 0.4 keV, maximum plasma pressure 3.2 bar, and the plasma stream diameter 18 cm. The plasma pulse shape is approximately triangular, pulse duration 0.25 ms and the heat loads varied in the range (0.2…2.5) MJ/m2. A deformed W grade sample delivered from Plansee AG, was used for the plasma load tests. Cylindrical shaped specimens had been a diameter of 12 mm and a height of 5 mm [4]. An electric heater was installed at target’s back- side to keep the target temperature in the range T0 = (200…600) °C before plasma pulse. For temperature monitoring a calibrated thermocouple and an infrared pyrometer were used. All targets were exposed to perpendicular plasma stream. The energy density in plasma stream and surface heat load measured with a calorimeter. Surface analysis was carried out with an optical microscope MMR-4 equipped with a CCD camera and Scanning Electron Microscopy (SEM) JEOL JSM-6390. The so called ‘ϑ-2ϑ scans’ with X-ray diffraction technique (XRD) of exposed targets were performed using a monochromatic Kα line of Cu anode radiation [7]. Diffraction peaks intensity, their profiles, and their angular positions were analyzed for estimation the macrostrain and the lattice parameters. 3. EXPERIMENTAL RESULTS 3.1. FEATURES PLASMA-SURFACE INTERACTION IN QSPA Kh-50 In our previous experiments it was demonstrated that tungsten melting threshold under QSPA Kh-50 exposures is (0.56…0.6) MJ/m2. The evaporation onset is estimated as 1.1 MJ/m2 [2]. For combined W-C targets the melting and evaporation was not achieved under the plasma exposures with fixed energy density. Enhanced evaporation of carbon (carbon evaporation threshold (0.4…0.45) MJ/m2) results in additional shielding of tungsten surface by C cloud. It protects W surface from the evaporation even for essentially increased energy density of impacting plasma [6]. Calorimetric measurements demonstrate that even for plasma exposures, which not result in the tungsten melting, the absorbed heat load is not more 60% of the impact plasma energy. The stopped plasma layer, formed from the head of the plasma stream, ceases to be completely transparent for subsequently impacting plasma mailto:makhlay@ipp.kharkov.ua 58 ions [2, 6]. This layer of cold plasma is responsible for decreasing part of incident plasma energy which is delivered to the surface. In recent studies for inclined exposure of the different targets, diminution of energy density delivered to surface has been observed with decrease of incidence angle (Fig. 1). 0 30 60 90 W W+C C 1.5 1.0 0.5 α q, M J/ m 2 α, degree 0.0 Plasma stream Fig.1. Heat load to the target surface vs. incidence angle of impacting plasma stream. Plasma stream energy density is 2.4 MJ/m2 3.2. CRACKING THRESHOLDS ANALYSIS Cracking development is characterized by measured threshold load and threshold target temperature, which determine the existing region of W performance without cracks. The energy threshold for tungsten cracking development is found to be ~0.3 J/m2 for QSPA Kh-50 pulse. The Ductile Brittle Transition Temperature (DBTT) is experimentally estimated. The Ductile Brittle Transition (DBT) occurs in the temperature range of 200 ºC TDBTT < 300 º . For initial temperature T0 > 300 °C no major cracks are formed on the exposed surface. Major cracks network forms only in cases of initial target temperatures below DBTT. Mesh of cells of major crack network is achieved (0.8…1.3) mm for near the center of the spot (Fig. 2). Fig. 2. SEM image of major crack network on tungsten surface after 5 pulses of 0.45 MJ/m2, T0 = 200 °C Intergranular micro-cracks appear after plasma exposition with heat load above melting threshold. Typical cell sizes of intergranular micro-cracks network are 10 to 80 µm. Most of cells are within (10…40) µm, which corresponds to the grain size of this W grade (Fig. 3). The micro-cracks propagate along the grain boundaries completely surrounding the grains. The typical width of intergranular cracks is not exceeded 1 µm. Fine cracks are developed in rather thin surface layer ~ (5…10) µm. Major cracks are much deeper (Fig. 4). Appearance of pores in some regions of surface layer can be caused by expansion of macro-cracks mesh and losses of tungsten grains in result of plasma impacts. Fig. 3. SEM image of micro cracks network on tungsten surface after 5 plasma pulses of 0.75 MJ/m2, T0 = 600 °C Fig. 4. Cross-section of tungsten target preheated at T0 = 200 °C and exposed with 10 pulses of 0.75 MJ/m2 3.3. RESIDUAL STRESSES IN TUNGSTEN AFFECTED BY PLASMA STREAMS The XRD diffraction analysis has confirmed absence of material phases built of impurities. Only W lines on the surface and in deeper layers were observed. This is important indication of plasma and target purity. Plasma irradiation results in a symmetrical tensile stress in thin subsurface layer. Rather weak dependencies of residual stresses on the initial temperature and the irradiation dose were obtained for plasma exposures with heat load of 0.2 MJ/m2. The values of residual stresses ≈ 160…180) MPa. The residual stress of 314 MPa appears in the surface preheated to T0 = 200 °C and exposed by single plasma pulse of 0.45 MJ/m2. If T0 overcomes the DBTT point the stress drops down to 250 MPa. Increasing the number of plasma pulses leads to some saturation of residual stress which does not depend on T0 (Fig. 5). Single pulse irradiation of W surface preheated at 200 0C with the heat load above the melting threshold 0.75 MJ/m2 led to the absolute maximal residual stress 390 MPa. Preheating of tungsten at the temperature larger than 400 0C causes the saturation of the residual stress in tungsten on the level of 300 MPa. In the course of 5 plasma pulses the residual stress linearly decreases from 59 362 MPa down to 200 MPa with rising of initial surface temperature from 200 up to 600 0C (see Fig. 5). 0 200 400 600 800 0 100 200 300 400 500 2 1 R es id ua l s tr es se s ( M Pa ) Temperature (C) Fig.5. Residual stresses in tungsten targets exposed with five QSPA plasma pulses of 0.45 MJ/m2 (1) and 0.75 MJ/m2(2) versus the initial bulk temperature 4. CONCLUSIONS 1. Features of tungsten erosion under repetitive plasma heat loads up to 1.1 MJ/m2 lasting 0.25 ms, which are relevant to ITER Type I ELMs, has been investigated. 2. Influence of target inclination and neighborhood W and C as divertor components on the material response to the repetitive plasma heat loads was analyzed. 3. The energy threshold for cracking development is found to be ~0.3 J/m2 for plasma pulse of 0.25 ms duration with triangular pulse shape. 4. The Ductile-to-Brittle Transition occurs in the temperature range of 200 ºC TDBTT < 300 º . For initial target temperature T0 > 300 C no major cracks are formed on the exposed surface. 5. Major cracks network forms only if initial target temperature is below DBTT. The intergranular micro- cracks network appears under heat loads above the melting threshold. 6. Performed measurements demonstrate that the residual stress does not depend practically on initial target temperature and it significantly grows with increasing thermal loads. This work is supported in part by STCU project # P405 REFERENCES 1. J. Roth, et al. // Journal of Nuclear Materials. 2009, v. 390–391, p. 1-9. 2. V.I. Tereshin, et al. // Plasma Physics Controlled Fusion. 2007, v. 49, p. A231-A239. 3. N. Klimov, et al. // Journal of Nuclear Materials. 2009, v. 390–391, p. 721–726. 4. T. Hirai, et al. // Journal of Nuclear Materials. 2009, v. 390–391, p. 751–754. 5. I.E. Garkusha, et al. // Physica Scripta. 2009, v. T138, 014054 (doi:10.1088/0031-8949/2009/T138/014054). 6. I.E. Garkusha, et al. // Journal of Nuclear Materials. 2009, v. 386–388, p. 127-131. 7. V.A. Makhlaj, et al. // Physica Scripta. 2009, v. T138, 014060 (doi: 10.1088/0031-8949/2009/T138/014060). 8. V.A. Makhlay, et al. // Physica Scripta. 2007. v. T128, p. 239-241. Article received 29. 10. 2010 ITER , ELM, -50 . , .E. , . , , . , . , . , . , . , A.T. , . , , , ELM ITER , -50 2,5 2 0,25 . ~0,3 2. ( ) , ITER . ( 1,3 ) , . ( ) . , ELM, -50 . , . , . , , I. . , . , . , . , . , A.T. , . , , ELM , , -50 2,5 2 0,25 . ~0,3 2. ( ) , ITER . ( 1,3 ) , . ( ) . . .
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institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
issn 1562-6016
language English
last_indexed 2025-12-07T17:21:42Z
publishDate 2010
publisher Національний науковий центр «Харківський фізико-технічний інститут» НАН України
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spelling Makhlaj, V.A.
Garkusha, I.E.
Aksenov, N.N.
Kulik, N.V.
Landman, I.S.
Linke, J.
Medvedev, A.V.
Malykhin, S.V.
Chebotarev, V.V.
Pugachev, A.T.
Tereshin, V.I.
2011-02-26T20:57:28Z
2011-02-26T20:57:28Z
2010
HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50 / V.A. Makhlaj, I.E. Garkusha, N.N. Aksenov, N.V. Kulik, I.S. Landman, J. Linke, A.V. Medvedev, S.V. Malykhin, V.V. Chebotarev, A.T. Pugachev, V.I. Tereshin // Вопросы атомной науки и техники. — 2010. — № 6. — С. 57-59. — Бібліогр.: 8 назв. — англ.
1562-6016
https://nasplib.isofts.kiev.ua/handle/123456789/17458
Performed studies of plasma-surface interaction include measurements of plasma energy deposited to the material surface and determination of tungsten cracking threshold during repetitive ITER ELM-like plasma exposures in QSPA Kh-50 with plasma pulses of energy density up to 2.5 MJ/m2 and duration of 0.25 ms. The energy threshold for tungsten cracking development is found to be ~0,3 MJ/m2. The Ductile-to-Brittle Transition Temperature (DBTT) is experimentally estimated for ITER relevant tungsten grade. Major crack network (cells size up to 1.3 mm) forms only in cases of initial target temperatures below DBTT. Intergranular micro-cracks network (size of cells corresponds to the grain size) appears under heat loads after melting threshold.
en
Національний науковий центр «Харківський фізико-технічний інститут» НАН України
ИТЭР и приложения для термоядерного реактора
HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50
Тестирование мощными потоками плазмы материалов дивертора ITER в условиях, соответствующих ELM, на КСПУ Х-50
Article
published earlier
spellingShingle HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50
Makhlaj, V.A.
Garkusha, I.E.
Aksenov, N.N.
Kulik, N.V.
Landman, I.S.
Linke, J.
Medvedev, A.V.
Malykhin, S.V.
Chebotarev, V.V.
Pugachev, A.T.
Tereshin, V.I.
ИТЭР и приложения для термоядерного реактора
title HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50
title_alt Тестирование мощными потоками плазмы материалов дивертора ITER в условиях, соответствующих ELM, на КСПУ Х-50
title_full HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50
title_fullStr HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50
title_full_unstemmed HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50
title_short HIgh heat flux plasma testing of ITER divertor materials under ELM relevant conditions in QSPA Kh-50
title_sort high heat flux plasma testing of iter divertor materials under elm relevant conditions in qspa kh-50
topic ИТЭР и приложения для термоядерного реактора
topic_facet ИТЭР и приложения для термоядерного реактора
url https://nasplib.isofts.kiev.ua/handle/123456789/17458
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