In situ scanning electron microscopy study of fatigue crack propagation

The fatigue crack propagation rate is influenced by various mechanisms at the very vicinity of the crack tip, e.g., local plasticity and/or creep, microcracking, crack branching, and crack closure induced by plasticity and roughness. To study these mechanisms and their influence on crack propagation...

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Опубліковано в: :Проблемы прочности
Дата:2008
Автори: Jacobsson, L., Persson, C., Melin, S.
Формат: Стаття
Мова:Англійська
Опубліковано: Інститут проблем міцності ім. Г.С. Писаренко НАН України 2008
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Онлайн доступ:https://nasplib.isofts.kiev.ua/handle/123456789/48418
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Цитувати:In situ scanning electron microscopy study of fatigue crack propagation / L. Jacobsson, C. Persson, S. Melin // Проблемы прочности. — 2008. — № 1. — С. 159-162. — Бібліогр.: 5 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
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author Jacobsson, L.
Persson, C.
Melin, S.
author_facet Jacobsson, L.
Persson, C.
Melin, S.
citation_txt In situ scanning electron microscopy study of fatigue crack propagation / L. Jacobsson, C. Persson, S. Melin // Проблемы прочности. — 2008. — № 1. — С. 159-162. — Бібліогр.: 5 назв. — англ.
collection DSpace DC
container_title Проблемы прочности
description The fatigue crack propagation rate is influenced by various mechanisms at the very vicinity of the crack tip, e.g., local plasticity and/or creep, microcracking, crack branching, and crack closure induced by plasticity and roughness. To study these mechanisms and their influence on crack propagation rate during different loadings, in situ scanning electron microscope studies have been performed. Throughout the load cycles images were taken and analyzed with an image analysis technique to measure the displacements around the crack tip. The obtained data can be used to determine compliance curves at any point along the crack, crack shapes, and the displacementfield in the crack tip vicinity. The technique has been used to analyze which mechanisms of crack propagation are realized during, e.g., fatigue with overloads, and thermomechanical fatigue. The results were compared with resultsfrom measurements using the direct currentpotential drop technique, and it was found that various load conditions promote different mechanisms for crack propagation. Скорость роста усталостной трещины (РУТ) определяется различными механизмами, реализуемыми в окрестности вершины тре­щины. Для изучения этих механизмов и их влияния на скорость РУТ для различных режимов нагружения были проведены иссле­дования in situ с помощью электронного ска­нирующего микроскопа. Микрофотографии, получаемые во время циклического нагру­жения, анализировались с помощью мето­дики обработки изображений с целью изме­рения перемещений в окрестности вершины трещины. Полученные результаты использо­вались для построения кривых податли­вости для любой точки на линии трещины, определения ее формы и поля перемещений вокруг вершины. По данной методике исследовались механизмы РУТ, реализуемые, в частности, при циклическом нагружении с перегрузками и термомеханической уста­лости. Полученные результаты сравнива­лись с данными измерений по методике падения потенциала. При этом было уста­новлено, что разным условиям нагружения соответствуют различные механизмы РУТ.
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fulltext UDC 539. 4 I n S itu S c a n n in g E le c tr o n M ic r o s c o p y S tu d y o f F a t ig u e C r a c k P r o p a g a t io n L . J a co b sso n ,1a C . P ersso n ,1b and S. M elin 2,c 1 Division o f Materials Engineering, Lund University, Lund, Sweden 2 Division o f Mechanics, Lund University, Lund, Sweden a lars.jacobsson@material.lth.se, b christer.persson@material.lth.se, c solveig.melin@mek.lth.se The fatigue crack propagation rate is influenced by various mechanisms at the very vicinity o f the crack tip, e.g., local plasticity and/or creep, microcracking, crack branching, and crack closure induced by plasticity and roughness. To study these mechanisms and their influence on crack propagation rate during different loadings, in situ scanning electron microscope studies have been performed. Throughout the load cycles images were taken and analyzed with an image analysis technique to measure the displacements around the crack tip. The obtained data can be used to determine compliance curves at any point along the crack, crack shapes, and the displacement field in the crack tip vicinity. The technique has been used to analyze which mechanisms o f crack propagation are realized during, e.g., fatigue with overloads, and thermomechanical fatigue. The results were compared with results from measurements using the direct current potential drop technique, and it was found that various load conditions promote different mechanisms fo r crack propagation. K e y w o rd s : fatigue, crack propagation, scanning electron m icroscope, crack shape, crack closure, potential drop. In trod u ction . It is o f interest to study the material in the crack tip v icin ity to understand the effects o f material p lasticity around the crack tip, roughness o f the crack faces, microstructure, stresses, and deform ations, on the crack propagation. Elber [1, 2] introduced the concept o f crack closure where the m axim um stress level at the crack tip is critical. The m axim um load, is calculated from the closure level, w here the crack tip is under zero load, and the applied stress intensity factor range. To m easure the crack closure load level, a number o f different m easurem ent techniques are used. Song and Shieh [3] used the direct current potential drop technique to find the crack closure level, whereas the A ST M E 647-99 [4] recom m ends to apply the crack mouth opening displacement. A lso, there are different techniques using m icroscope im ages to measure the displacements along the crack. The aim o f this study w as to determine the deform ations along the crack, and how the deform ations are affected by the different crack propagation m echanism s. H igh resolution im ages from an in-situ scanning electron m icroscope w as used to measure deform ations at the crack tip vicinity, and the potential drop technique w as used to m easure the contact betw een the crack surfaces. E xp er im en ta l Setup. The fatigue crack propagation experim ents were performed w ithin a scanning electron m icroscope (SEM ), using a sm all electrically driven load stage to perform the load cycles, also described by A ndersson et al. [5]. The test specim ens had dim ensions o f 7 0 x 1 0 m m and w ere cut from 0.5 m m Inconel 718 foil. The specim ens w ere prepared w ith a single-edge-notch tension (SE N T) crack, that w as pre-cracked in a servohydraulic load frame to a length o f 0 .7 -1 .0 mm. The specim ens were etched to produce a recognizable pattern on the surface o f the specim en for the SEM observations. The specim ens w ere prepared w ith thin w ires w elded at the crack m outh to measure the electrical potential drop signal over the crack. A direct current o f 1.0 A w as passed through the specim en and the potential drop signal w as am plified before saved in the computer. The crack propagation rate and the crack closure leve l were determined. A summary o f the performed experim ents is found in Table 1. © L. JA C O B SSO N , C. PER SSO N , S. M ELIN , 2008 ISSN 0556-171X. Проблемы прочности, 2008, № 1 159 mailto:lars.jacobsson@material.lth.se mailto:christer.persson@material.lth.se mailto:solveig.melin@mek.lth.se L. Jacobsson, C. Persson, and S. Melin T a b l e 1 Experimental Conditions for the Four Crack Propagation Experiments Experiment a, /im AK, MPa • m1/2 A K eff, MPa • m1/2 R ^ min / ̂ max i ■ 740 16.6 3.1 0.01 ii ▼ 945 19.7 10.0 0.01 iii ▲ 1673 43.3 26.3 0.01 iv • 1764 65.0 42.0 0.02 Im age A n a lysis M eth od . A n ew im age analysis m ethod w as developed to measure displacements in the crack tip vicinity from high resolution SEM im ages. Images were taken along the crack throughout the loading cycles. The displacements betw een different images w ere determ ined using a cross-correlation function that recognized a selected area o f one im age in another im age, taken at a different load. The area w as p laced w ithin 2 -1 0 ,am from the crack, w here the deform ation w ithin the material w as negligib le. Com pliance curves and crack shapes were determ ined from the m easured displacem ent field. R esu lts and D iscu ssion . Crack shapes and com pliance curves were determined during a number o f experim ents w ith different loading histories. C om pliance curves from points at different distances from the crack tip are compared in Fig. 1. The com pliance curve m easured at the crack mouth show ed neglig ib le influence from the plastic zone, and had a sm all knee at a higher load than the com pliance curves m easured at the crack tip, that show ed clear effects from the plastic zone and closure o f the crack surfaces. The knee on the curves from the potential drop (PD ) m easurem ents show ed in Fig. 2a, indicates the closure level. A bove this level the crack w as fu lly open and the change in electrical conductivity w as on ly due to the high stresses in front o f the crack, and b elow this level the contact betw een the crack surfaces increased with decreasing load. The load level at the knee on the PD -curves w as higher than that at the knee on the com pliance curves m easured at the crack mouth. Fig. 1. Compliance curves measured at three different distances from the crack tip: ( • ) 2 ^m; (A ) 20 ,Mm; (■ ) at the crack mouth. The crack shape obtained by linear elastic fracture m echanics (LEFM) considerations does not alw ays describe the true crack shape w e ll because o f the influence from the plastic zone and the microstructure. The LEFM solutions, as w ell as crack shapes com pensated for closure levels from com pliance curves and PD m easurem ents, are show n in Fig. 3. The LEFM solution w ill be the sam e, independent o f the closure level w hen the 160 ISSN 0556-171X. npoôëeMbi npounocmu, 2008, N 1 In Situ Scanning Electron Microscopy Study Fig. 2. Compliance curve with closure level at 1200 N (a) and the corresponding PD-curve with closure level at 1700 N (b) for K max = 65 MPa • m1/2, R = 0.02, overload ratio 1.26, a = 1.8 mm, specimen thickness 0.5 mm, and displacements measured 15 /im from the crack tip. (Experiment iv.) x icT1* о о uLi______ c______ c______ c______ c______ i______ a -3 -2,5 -2 -1.5 -1 -0.5 a Dist from crack tip (m) x kt4 Fig. 3. Experimental results are compensated for the effective stress intensity factor range measured from the compliance curve (▼) and from the PD signal (O). (Experiment iv. The opening displacements divided by the effective stress intensity factor range. The solid line shows the LEFM solution.) i и* * 11“ Dist. from crack tip (m) xiC® Dist fromcraDk lip (m) x Kf® a b Fig. 4. Crack shapes (a) and ^-deformations (b) divided by effective stress intensity factor range versus distance from crack tip for the four experiments. (Solid line is the LEFM solution.) ISSN 0556-171X. Проблемы прочности, 2008, N 1 161 L. Jacobsson, C. Persson, and S. Melin displacem ent divided by the effective stress intensity factor range is plotted. W hen the experim ental results were divided by the closure levels m easured from the com pliance curves and the PD-curves, the results diverged (Fig. 3). In Fig. 4a, the crack shapes are plotted for four different experim ents (Table 1). This close to the crack tip, the microstructure and the change in crack direction affects the crack shape. In Fig. 4b, the deform ation w as divided w ith the effective stress intensity factor found from com pliance curves. The results show ed sim ilarities betw een the four experim ents and also the LEFM solution w as c lose to the experim ental results. The crack tip is show n in Fig. 5. Fig. 5. SEM image o f the crack tip at maximum load. (Experiment iii.) C on clusions. Experim ents have been performed w ithin a SEM and the im ages were used to determine deform ations in the v icin ity o f the crack tip. C om pliance curves were determ ined and com pared w ith results from PD m easurem ents. The PD measurem ents gave higher values for the crack closure load than the com pliance m easurem ents. W hen the experim ental results, com pensated for crack closure w ere com pared w ith the LEFM solution, the crack shapes at the crack tip v icin ity becam e comparable even w hen the crack shapes w ere irregular due to the microstructural variations. Acknowledgments. The authors give their acknowledgements to the Swedish Gas Turbine Center for the financial support. 1. W. Elber, Eng. Fract. M ech, 2, 37-45 (1970). 2. W. Elber, in: Damage Tolerance in Aircraft Structures, ASTM STP 486 (1971), pp. 230-242. 3. P. S. Song and Y. L. Shieh, Int. J. Fatigue, 26, 429-436 (2004). 4. Standard Test Method fo r Measurement o f Fatigue Crack Growth Rates, ASTM E647-99 (1995). 5. M. Andersson, C. Persson, and S. Melin, Int. J. Fatigue, 28, 1059-1068 (2006). Received 28. 06. 2007 162 ISSN 0556-171X. npo6neMbi npouHocmu, 2008, № 1
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institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
issn 0556-171X
language English
last_indexed 2025-12-07T17:08:46Z
publishDate 2008
publisher Інститут проблем міцності ім. Г.С. Писаренко НАН України
record_format dspace
spelling Jacobsson, L.
Persson, C.
Melin, S.
2013-08-19T13:19:55Z
2013-08-19T13:19:55Z
2008
In situ scanning electron microscopy study of fatigue crack propagation / L. Jacobsson, C. Persson, S. Melin // Проблемы прочности. — 2008. — № 1. — С. 159-162. — Бібліогр.: 5 назв. — англ.
0556-171X
https://nasplib.isofts.kiev.ua/handle/123456789/48418
539.4
The fatigue crack propagation rate is influenced by various mechanisms at the very vicinity of the crack tip, e.g., local plasticity and/or creep, microcracking, crack branching, and crack closure induced by plasticity and roughness. To study these mechanisms and their influence on crack propagation rate during different loadings, in situ scanning electron microscope studies have been performed. Throughout the load cycles images were taken and analyzed with an image analysis technique to measure the displacements around the crack tip. The obtained data can be used to determine compliance curves at any point along the crack, crack shapes, and the displacementfield in the crack tip vicinity. The technique has been used to analyze which mechanisms of crack propagation are realized during, e.g., fatigue with overloads, and thermomechanical fatigue. The results were compared with resultsfrom measurements using the direct currentpotential drop technique, and it was found that various load conditions promote different mechanisms for crack propagation.
Скорость роста усталостной трещины (РУТ) определяется различными механизмами, реализуемыми в окрестности вершины тре­щины. Для изучения этих механизмов и их влияния на скорость РУТ для различных режимов нагружения были проведены иссле­дования in situ с помощью электронного ска­нирующего микроскопа. Микрофотографии, получаемые во время циклического нагру­жения, анализировались с помощью мето­дики обработки изображений с целью изме­рения перемещений в окрестности вершины трещины. Полученные результаты использо­вались для построения кривых податли­вости для любой точки на линии трещины, определения ее формы и поля перемещений вокруг вершины. По данной методике исследовались механизмы РУТ, реализуемые, в частности, при циклическом нагружении с перегрузками и термомеханической уста­лости. Полученные результаты сравнива­лись с данными измерений по методике падения потенциала. При этом было уста­новлено, что разным условиям нагружения соответствуют различные механизмы РУТ.
The authors give their acknowledgements to the Swedish Gas Turbine Center for the financial support.
en
Інститут проблем міцності ім. Г.С. Писаренко НАН України
Проблемы прочности
Научно-технический раздел
In situ scanning electron microscopy study of fatigue crack propagation
Исследование in situ роста усталостной трещины с помощью электронного сканирующего микроскопа
Article
published earlier
spellingShingle In situ scanning electron microscopy study of fatigue crack propagation
Jacobsson, L.
Persson, C.
Melin, S.
Научно-технический раздел
title In situ scanning electron microscopy study of fatigue crack propagation
title_alt Исследование in situ роста усталостной трещины с помощью электронного сканирующего микроскопа
title_full In situ scanning electron microscopy study of fatigue crack propagation
title_fullStr In situ scanning electron microscopy study of fatigue crack propagation
title_full_unstemmed In situ scanning electron microscopy study of fatigue crack propagation
title_short In situ scanning electron microscopy study of fatigue crack propagation
title_sort in situ scanning electron microscopy study of fatigue crack propagation
topic Научно-технический раздел
topic_facet Научно-технический раздел
url https://nasplib.isofts.kiev.ua/handle/123456789/48418
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