Microwave assisted synthesis of pyrimido[4,5-d]pyrimidine derivatives in dry media
Pyrimido[4,5-d]pyrimidine derivatives were synthesized by using an efficient, facile and solvent-free procedure. Here, a non-conventional synthetic procedure has been developed where solid support of alumina is used as energy transfer medium under microwave irradiation (MWI) which devoids hazards of...
Gespeichert in:
| Datum: | 2009 |
|---|---|
| Hauptverfasser: | , , , , |
| Format: | Artikel |
| Sprache: | English |
| Veröffentlicht: |
Інститут молекулярної біології і генетики НАН України
2009
|
| Online Zugang: | https://nasplib.isofts.kiev.ua/handle/123456789/7368 |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| Назва журналу: | Digital Library of Periodicals of National Academy of Sciences of Ukraine |
| Zitieren: | Microwave assisted synthesis of pyrimido[4,5-d]pyrimidine derivatives in dry media / A.H. Kategaonkar, S.A. Sadaphal, K.F. Shelke, B.B. Shingate, M.S. Shingare // Ukrainica Bioorganica Acta. — 2009. — Т. 7, № 1. — С. 3-7. — Бібліогр.: 19 назв. — англ. |
Institution
Digital Library of Periodicals of National Academy of Sciences of Ukraine| Zusammenfassung: | Pyrimido[4,5-d]pyrimidine derivatives were synthesized by using an efficient, facile and solvent-free procedure. Here, a non-conventional synthetic procedure has been developed where solid support of alumina is used as energy transfer medium under microwave irradiation (MWI) which devoids hazards of solution phase reactions. The reaction time has been brought down from minutes to seconds with improved yield as compared to reported method. |
|---|