Структура молекулярного димерного алкоксокомплексу хрому (ІІІ) з диметил-N-трихлороацетиламідофосфатом

A new coordination compound of chromium (III) with dimethyl-N-trichloroacetylamidophosphate (L¯ = Cl3CC(O)NP(O)(OCH3)2) has been obtained. Based on IR data, the bidentate coordination mode of the carbacylamidophosphate ligand is suggested. The centrosymmetric bi-nuclear complex [Cr2(L)4(μ2−OCH3)2] h...

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Bibliographic Details
Date:2008
Main Authors: Труш, Є.А., Труш, В.А., Домасевич, К.В., Амірханов, В.М.
Format: Article
Language:Ukrainian
Published: Видавничий дім "Академперіодика" НАН України 2008
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Online Access:https://nasplib.isofts.kiev.ua/handle/123456789/7495
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Journal Title:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Cite this:Структура молекулярного димерного алкоксокомплексу хрому (ІІІ) з диметил-N-трихлороацетиламідофосфатом / Є.А. Труш, В.А. Труш, К.В. Домасевич, В.М. Амiрханов // Доп. НАН України. — 2008. — № 12. — С. 130-135. — Бібліогр.: 14 назв. — укр.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
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Summary:A new coordination compound of chromium (III) with dimethyl-N-trichloroacetylamidophosphate (L¯ = Cl3CC(O)NP(O)(OCH3)2) has been obtained. Based on IR data, the bidentate coordination mode of the carbacylamidophosphate ligand is suggested. The centrosymmetric bi-nuclear complex [Cr2(L)4(μ2−OCH3)2] has molecular structure according to X-ray analysis. The phosphoramidic ligands are coordinated in a bidentate manner via oxygen atoms of phosphoryl and carbonyl groups, and the coordination polyhedra represent the cis-isomer. The coordination environment of the central ion possesses a distorted octahedral geometry with c.n. = 6. The polyhedron (CrO6) comprises 4O from two bidentate phosphorylic ligands and 2O from bridging methoxide ions.
ISSN:1025-6415