System of spectrally pure hydrogen inflow for Uragan-3M torsatron

The used today system of hydrogen inflow into Uragan-3M torsatron (U-3M) vacuum chamber does not provide the needed purity of hydrogen during plasma experiments. In view of this, the simple construction of a diffusion Pdmembrane module system for spectrally pure hydrogen inflow was suggested and sim...

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Опубліковано в: :Вопросы атомной науки и техники
Дата:2000
Автори: Glazunov, G.P., Volkov, E.D., Baron, D.I.
Формат: Стаття
Мова:English
Опубліковано: Національний науковий центр «Харківський фізико-технічний інститут» НАН України 2000
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Онлайн доступ:https://nasplib.isofts.kiev.ua/handle/123456789/78495
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Цитувати:System of spectrally pure hydrogen inflow for Uragan-3M torsatron / G.P. Glazunov, E.D. Volkov, D.I. Baron // Вопросы атомной науки и техники. — 2000. — № 6. — С. 50-51. — Бібліогр.: 3 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
id nasplib_isofts_kiev_ua-123456789-78495
record_format dspace
spelling Glazunov, G.P.
Volkov, E.D.
Baron, D.I.
2015-03-18T16:06:45Z
2015-03-18T16:06:45Z
2000
System of spectrally pure hydrogen inflow for Uragan-3M torsatron / G.P. Glazunov, E.D. Volkov, D.I. Baron // Вопросы атомной науки и техники. — 2000. — № 6. — С. 50-51. — Бібліогр.: 3 назв. — англ.
1562-6016
https://nasplib.isofts.kiev.ua/handle/123456789/78495
533.9
The used today system of hydrogen inflow into Uragan-3M torsatron (U-3M) vacuum chamber does not provide the needed purity of hydrogen during plasma experiments. In view of this, the simple construction of a diffusion Pdmembrane module system for spectrally pure hydrogen inflow was suggested and simulation experiments with experimental module were carried out. The tests on the special stand and in the U-3M vacuum vessel have showed such performances of the experimental module at T = 650°C and 1 at. hydrogen pressure: power for heating is ≈200 watt, hydrogen flow through membrane Q ≈ 1 Torr.l/s (specific hydrogen flow through membrane q ≈ 5.10-2 Torr.l/s.cm2). The preliminary results obtained in this work have given the possibility to start the work design and construction of the system for inflow of spectrally pure hydrogen for the U-3M torsatron. Some details of this system are presented.
en
Національний науковий центр «Харківський фізико-технічний інститут» НАН України
Вопросы атомной науки и техники
Magnetic confinement
System of spectrally pure hydrogen inflow for Uragan-3M torsatron
Article
published earlier
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
title System of spectrally pure hydrogen inflow for Uragan-3M torsatron
spellingShingle System of spectrally pure hydrogen inflow for Uragan-3M torsatron
Glazunov, G.P.
Volkov, E.D.
Baron, D.I.
Magnetic confinement
title_short System of spectrally pure hydrogen inflow for Uragan-3M torsatron
title_full System of spectrally pure hydrogen inflow for Uragan-3M torsatron
title_fullStr System of spectrally pure hydrogen inflow for Uragan-3M torsatron
title_full_unstemmed System of spectrally pure hydrogen inflow for Uragan-3M torsatron
title_sort system of spectrally pure hydrogen inflow for uragan-3m torsatron
author Glazunov, G.P.
Volkov, E.D.
Baron, D.I.
author_facet Glazunov, G.P.
Volkov, E.D.
Baron, D.I.
topic Magnetic confinement
topic_facet Magnetic confinement
publishDate 2000
language English
container_title Вопросы атомной науки и техники
publisher Національний науковий центр «Харківський фізико-технічний інститут» НАН України
format Article
description The used today system of hydrogen inflow into Uragan-3M torsatron (U-3M) vacuum chamber does not provide the needed purity of hydrogen during plasma experiments. In view of this, the simple construction of a diffusion Pdmembrane module system for spectrally pure hydrogen inflow was suggested and simulation experiments with experimental module were carried out. The tests on the special stand and in the U-3M vacuum vessel have showed such performances of the experimental module at T = 650°C and 1 at. hydrogen pressure: power for heating is ≈200 watt, hydrogen flow through membrane Q ≈ 1 Torr.l/s (specific hydrogen flow through membrane q ≈ 5.10-2 Torr.l/s.cm2). The preliminary results obtained in this work have given the possibility to start the work design and construction of the system for inflow of spectrally pure hydrogen for the U-3M torsatron. Some details of this system are presented.
issn 1562-6016
url https://nasplib.isofts.kiev.ua/handle/123456789/78495
citation_txt System of spectrally pure hydrogen inflow for Uragan-3M torsatron / G.P. Glazunov, E.D. Volkov, D.I. Baron // Вопросы атомной науки и техники. — 2000. — № 6. — С. 50-51. — Бібліогр.: 3 назв. — англ.
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first_indexed 2025-11-25T20:39:24Z
last_indexed 2025-11-25T20:39:24Z
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fulltext UDC 533.9 50 Problems of Atomic Science and Technology. 2000. № 6. Series: Plasma Physics (6). p. 50-51 SYSTEM OF SPECTRALLY PURE HYDROGEN INFLOW FOR URAGAN-3M TORSATRON G.P. Glazunov, E.D. Volkov, D.I. Baron Institute of Plasma Physics of NSC KhIPT, 61108 Kharkov, Ukraine e-mail: glazunov@ipp.kharkov.ua The used today system of hydrogen inflow into Uragan-3M torsatron (U-3M) vacuum chamber does not provide the needed purity of hydrogen during plasma experiments. In view of this, the simple construction of a diffusion Pd- membrane module system for spectrally pure hydrogen inflow was suggested and simulation experiments with experimental module were carried out. The tests on the special stand and in the U-3M vacuum vessel have showed such performances of the experimental module at T = 650°C and 1 at. hydrogen pressure: power for heating is ≈200 watt, hydrogen flow through membrane Q ≈ 1 Torr.l/s (specific hydrogen flow through membrane q ≈ 5.10-2 Torr.l/s.cm2). The preliminary results obtained in this work have given the possibility to start the work design and construction of the system for inflow of spectrally pure hydrogen for the U-3M torsatron. Some details of this system are presented. 1. Introduction The today system of hydrogen inflow into Uragan- 3M torsatron (U-3M) vacuum chamber was made of hydrogen inlet from a high pressure vessel through automatic inlet system. However, even if the high purity hydrogen is contain in a high pressure vessel, such system does not provide the needed purity of hydrogen during plasma experiments (usually about a few percents of impurities) . So the value of the most experimental results comes lower and a new system for spectrally pure hydrogen inflow is needed. It is the main reason that in this work the new diffusion Pd-membrane module system for spectrally pure hydrogen inflow was suggested and the simulation experiments with the experimental module of such system were carried out. 2. Conception and design The usually used for spectrally pure hydrogen inflow Pd-membranes have thickness about 1 mm ( in order to provide the long life time and reliability). However, it is the difficult task to release the high required hydrogen flow Q ( up to 5 Torr.l/s) for the U-3M by the use of such membranes (one must remember that Q ~ d-1). In this work the utilizing of the rather thin Pd-membrane 0.1-0.25 mm thickness is suggested. And, in order to provide the required reliability, the special procedure of membrane heating and pumping of dissolved hydrogen is anticipated. This excludes the possibility of membrane disruption due to α-β transition in Pd. To exclude of heavy Pd-atom input into plasma volume it is suggested to use the TiN-coated palladium membranes. The block-scheme of suggested system is shown in Fig.1. System comprises a block of diffusion membranes, which includes six diffusion modules, each of other has independent heating system. There are also the hydrogen pressure and temperature control systems, and pumping system to provide the functioning of diffusion modules. If it is needed the automatic systems can be used to keep the temperature and hydrogen pressure regime of diffusion module (pushed in the Fig.1). Also one can use the scheme with hydrogen generation block through the use of a palladium membrane and ethyl alcohol vapors. It was demonstrated earlier [1] that at an optimum ethyl alcohol vapor pressure and a membrane temperature such hydrogen generation scheme can provide hydrogen flow about 1 Torr.l/s for one Pd-membrane with surface area ≈ 20 cm2 . But some additional investigations to be carried out to clarify the influence of carbon, releasing on the membrane surface due to ethyl vapor dehydration and thermal decomposition of ethylene, on the kinetics of hydrogen generation and penetration. 3. Experimental set-up The experimental module (Fig.2) comprises a diffusion membrane (Pd-99.98 grade pipes 0.6 cm in diameter, 19 cm length, 0.025 cm in thickness), which was hermetically brazed at the one end. The outer surface of pipe was presented to the vacuum chamber, while the inner surface was in contact with hydrogen of high pressure vessel. The experimental modules under studies were also with the similar palladium pipes coated with a 3-µm-thick TiN layer. The membrane was heated by directly running the current through it. The temperature was controlled by chromel-Copel thermocouple located inside the pipe. The tests of above mentioned diffusion module on the special stand, the scheme of which is similar to that described in [1] and in the U-3M vacuum vessel have showed such performances at T=650°C and 1 at. hydrogen pressure: power for heating is ≈200 watt, hydrogen flow through membrane Q ≈ 1 Torr.l/s (specific hydrogen flow through membrane q ≈ 5.10-2 Torr.l/s.cm2). The H2 pressure increase up to 2.10-5 Torr was observed in the U-3M vacuum chamber during such hydrogen inlet. Taking into account the net hydrogen pumping speed ~ 105 l/s in the U-3M vacuum chamber and ~ 5.10-4 Torr hydrogen pressure needed during experiments, the total number five/six of mentioned modules are necessary in order to get the required hydrogen flow 5 Torr.l/s into the U-3M vacuum chamber. The diffusion module performances can be mailto:glazunov@ipp.kharkov.ua 51 improved by utilizing of more thin (up to 0.1 mm in U- 3M) Pd-pipes with larger diameter as the membrane thickness d dependence of Q is Q ~ d-1. The hydrogen pressure dependence of hydrogen flow through membrane is Q ~ p0.5. More detail description of hydrogen behavior in Pd-membranes and TiN-coated Pd-membranes is given in [2,3]. Fig. 1. Block-scheme of experimental set-up Fig.2. Experimental diffusion module Conclusion The preliminary results obtained in this work has shown the principal possibility for creation of a work system of spectrally pure hydrogen inflow for the U- 3M torsatron . The nearest future steps in this direction will be the work design, construction and mounting of such system. References [1] G.P.Glazunov, E.D. Volkov, D.I. Baron. Study of low hydrogen flows into high-vacuum systems. Int. J. Hydrogen Energy. 1999, v. 24, p. 829-831. [2] G.P.Glazunov. Hydrogen permeation through palladium after hydrogen-thermal treatment and exposure to a plasma of glow discharge in hydrogen, helium and argon. J. Hydrogen Energy, 1997, v. 20 No 2/3, p. 263-268. [3] G.P.Glazunov, E.D. Volkov, V.P. Veremeenko et al. Erosion and outgassing behavior of TiN-coated plasma facing components of the Uragan-3M torsatron. 14th Int. Conf. on Plasma Surface Interactions in Controlled Fusion Devices, Rosenheim, Germany, May 22-26, 2000, Book of Abstracts, P-3.18, to be published in J. Nucl. Mater. H 2 Diffusion membrane block Uragan-3M vacuum chamber Pressure control system Pumping systemHeating system Hydrogen generation system Automatic pressure control Automatic temperature control Temperature control system Heating Diffusion membrane Thermocouple Insulator F Fig. 1. Block-scheme of experimental set-up