The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles

The isolated resonance of the nuclear reaction on impurity interstitials was used to investigate orientation effects. The method is shown to provide the best energy resolution in comparison with other methods. The ¹³C(p,γ) ¹⁴N reaction resonance at a proton energy of 1.7476 MeV was used to inves...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Datum:2005
Hauptverfasser: Shershnev, V.M., Skakun, N.A.
Format: Artikel
Sprache:English
Veröffentlicht: Національний науковий центр «Харківський фізико-технічний інститут» НАН України 2005
Schriftenreihe:Вопросы атомной науки и техники
Schlagworte:
Online Zugang:https://nasplib.isofts.kiev.ua/handle/123456789/81223
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Назва журналу:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Zitieren:The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles / V.M. Shershnev, N.A. Skakun // Вопросы атомной науки и техники. — 2005. — № 6. — С. 37-39. — Бібліогр.: 5 назв. — англ.

Institution

Digital Library of Periodicals of National Academy of Sciences of Ukraine
id nasplib_isofts_kiev_ua-123456789-81223
record_format dspace
spelling nasplib_isofts_kiev_ua-123456789-812232025-02-09T16:40:06Z The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles Метод ізольованого резонансу та електронні гальмові втрати енергії гіперканальованих частинок Метод изолированного резонанса и электронные тормозные потери энергии гиперканалированных частиц Shershnev, V.M. Skakun, N.A. Ядерная физика и элементарные частицы The isolated resonance of the nuclear reaction on impurity interstitials was used to investigate orientation effects. The method is shown to provide the best energy resolution in comparison with other methods. The ¹³C(p,γ) ¹⁴N reaction resonance at a proton energy of 1.7476 MeV was used to investigate the proton flux distribution in the (0001) plane channel of the single-crystal solution Re-0.4 at.%¹³C. Some special features of the γ-quantum yield of the reaction in relation to energy have been established. Electron energy losses of hyperchanneled protons were measured. It is demonstrated that the γ-quantum yield of the channeled proton-excited reaction is dependent on the amplitude of thermal vibrations of carbon atoms. Ізольований резонанс ядерної реакції на впроваджених атомах домішок використано для вивчення орієнтаційних ефектів. Показано, що цей метод дозволяє одержати краще енергетичне розрізнення у порів- нянні з іншими методами. Резонанс реакції ¹³C(p,γ) ¹⁴N, при енергії протонів 1,7476 МеВ, використовувався для дослідження розподілу потоку протонів у площинному каналі (0001) монокристалічного розчину Re- 0,4 ат.%¹³С. Встановлено особливості виходу γ-квантів реакції в залежності від енергії. Виміряно електронні втрати енергії гіперканальованих протонів. Показано, що вихід γ-квантів реакції, що збуджується канальованими протонами, залежить від амплітуди теплових коливань атомів вуглецю. Изолированный резонанс ядерной реакции на примесных атомах внедрения использован для изучения ориентационных эффектов. Показано, что этот метод позволяет получить лучшее энергетическое разрешение по сравнению с другими методами. Резонанс реакции ¹³C(p,γ) ¹⁴N, при энергии протонов 1,7476 МэВ, использовался для исследования распределения потока протонов в плоскостном канале (0001) монокристаллического раствора Re-0,4 ат.%¹³С. Установлены особенности выхода γ-квантов реакции в зависимости от энергии. Измерены электронные потери энергии гиперканалированных протонов. Показано, что выход γ- квантов реакции, возбуждаемой каналированными протонами, зависит от амплитуды тепловых колебаний атомов углерода. The work was done with partial support of Project X866 ЯMРT 2010. 2005 Article The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles / V.M. Shershnev, N.A. Skakun // Вопросы атомной науки и техники. — 2005. — № 6. — С. 37-39. — Бібліогр.: 5 назв. — англ. 1562-6016 PACS: 24.30.-v, 68.35.Dv, 68.35.Ln, 61.72.Ji https://nasplib.isofts.kiev.ua/handle/123456789/81223 en Вопросы атомной науки и техники application/pdf Національний науковий центр «Харківський фізико-технічний інститут» НАН України
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
language English
topic Ядерная физика и элементарные частицы
Ядерная физика и элементарные частицы
spellingShingle Ядерная физика и элементарные частицы
Ядерная физика и элементарные частицы
Shershnev, V.M.
Skakun, N.A.
The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles
Вопросы атомной науки и техники
description The isolated resonance of the nuclear reaction on impurity interstitials was used to investigate orientation effects. The method is shown to provide the best energy resolution in comparison with other methods. The ¹³C(p,γ) ¹⁴N reaction resonance at a proton energy of 1.7476 MeV was used to investigate the proton flux distribution in the (0001) plane channel of the single-crystal solution Re-0.4 at.%¹³C. Some special features of the γ-quantum yield of the reaction in relation to energy have been established. Electron energy losses of hyperchanneled protons were measured. It is demonstrated that the γ-quantum yield of the channeled proton-excited reaction is dependent on the amplitude of thermal vibrations of carbon atoms.
format Article
author Shershnev, V.M.
Skakun, N.A.
author_facet Shershnev, V.M.
Skakun, N.A.
author_sort Shershnev, V.M.
title The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles
title_short The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles
title_full The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles
title_fullStr The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles
title_full_unstemmed The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles
title_sort isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles
publisher Національний науковий центр «Харківський фізико-технічний інститут» НАН України
publishDate 2005
topic_facet Ядерная физика и элементарные частицы
url https://nasplib.isofts.kiev.ua/handle/123456789/81223
citation_txt The isolated resonance method for investigating orientation effects and electron energy losses of hyperchanneled particles / V.M. Shershnev, N.A. Skakun // Вопросы атомной науки и техники. — 2005. — № 6. — С. 37-39. — Бібліогр.: 5 назв. — англ.
series Вопросы атомной науки и техники
work_keys_str_mv AT shershnevvm theisolatedresonancemethodforinvestigatingorientationeffectsandelectronenergylossesofhyperchanneledparticles
AT skakunna theisolatedresonancemethodforinvestigatingorientationeffectsandelectronenergylossesofhyperchanneledparticles
AT shershnevvm metodízolʹovanogorezonansutaelektronnígalʹmovívtratienergíígíperkanalʹovanihčastinok
AT skakunna metodízolʹovanogorezonansutaelektronnígalʹmovívtratienergíígíperkanalʹovanihčastinok
AT shershnevvm metodizolirovannogorezonansaiélektronnyetormoznyepoteriénergiigiperkanalirovannyhčastic
AT skakunna metodizolirovannogorezonansaiélektronnyetormoznyepoteriénergiigiperkanalirovannyhčastic
AT shershnevvm isolatedresonancemethodforinvestigatingorientationeffectsandelectronenergylossesofhyperchanneledparticles
AT skakunna isolatedresonancemethodforinvestigatingorientationeffectsandelectronenergylossesofhyperchanneledparticles
first_indexed 2025-11-28T01:57:35Z
last_indexed 2025-11-28T01:57:35Z
_version_ 1849997460587413504
fulltext THE ISOLATED RESONANCE METHOD FOR INVESTIGATING ORIENTATION EFFECTS AND ELECTRON ENERGY LOSSES OF HYPERCHANNELED PARTICLES V.M. Shershnev, N.A. Skakun National Science Center “Kharkov Institute of Physics and Technology”, Kharkov, Ukraine e-mail: skakun@kipt.kharkov.ua The isolated resonance of the nuclear reaction on impurity interstitials was used to investigate orientation effects. The method is shown to provide the best energy resolution in comparison with other methods. The 13C(p,γ)14N reaction resonance at a proton energy of 1.7476 MeV was used to investigate the proton flux distribution in the (0001) plane channel of the single-crystal solution Re-0.4 at.%13C. Some special features of the γ-quantum yield of the reaction in relation to energy have been established. Electron energy losses of hyperchanneled protons were measured. It is demonstrated that the γ-quantum yield of the channeled proton-excited reaction is dependent on the amplitude of thermal vibrations of carbon atoms. PACS: 24.30.-v, 68.35.Dv, 68.35.Ln, 61.72.Ji 1. INTRODUCTION The basic facts about orientation effects at channeling of hydrogen and helium ions were obtained from the analysis of angular and energy distributions of particles scattered by the nuclei of crystal atoms [1]. In the narrow energy range, in the near-surface region of the crystal, at depths of up to ~ 6 wavelengths of particle trajectory oscillations, the scattering spectrum shows a fine structure. Therefore, in studies of a channeled particle flux in this region, stringent requirements are imposed on the energy resolution of the method. The two factors, namely, straggling (discrete statistical character of electron energy loss fluctuations in the medium) at the crystal in/out parts of the scattered particle trajectory and the energy resolution of the spectrometer, substantially restrict the experimental possibilities of the scattering method. This leads to the smoothing of spectra, blurring of their structure and, as a consequence, to ambiguities in the analysis of results [2]. To investigate the orientation effects, we offer an approach based on the use of isolated resonances of excitation functions of the reactions on the impurity interstitial and substitution atoms, which occupy certain positions in the crystal. 2. METHOD The property of many nuclear reactions is the presence of one or more peaks (resonances) in the plot showing the radiation yield (e.g., (p,γ) reaction) versus particle energy. These resonances are measured experimentally by varying the energy through its small increments with simultaneous measurement of the reaction yield for each energy value. At E0 > Eres, the particle loses its energy in the target until the energy attains the resonance value at the depth “x” in the “δx” element, where the reaction takes place. If the reaction is excited by channeled particles, the resonance radiation yield depends not only on the atom concentration in the “δx”. In this case, the yield is also dependent on many other factors: the flux distribution in the channel, the arrangement of atoms, on which the reaction is excited, electron energy losses of channeled particles, the energy straggling, the crystallographic direction, etc. The resolution of the elastic scattering method, without regard for both the geometry responsible for the solid acceptance angle of the detector and the target surface roughness, is given by the expression ( ) ( ) ( ) ( ) ( ) 22222 outinspcbmbs EEEEE δδδδ +++=∆ , (1) where δEbm is the beam energy straggling at entry into the crystal, δEspc is the spectrometer resolution, δEin, δEout denote the straggling before and after particle scattering in the target, respectively. 0 2 4 6 8 10 0 1 2 3 4 5 6 7 8 9 10 ∆ E (k eV ) Energy losses (keV) Fig. 1. Energy resolution of the backscattering method as a function of energy losses for the surface- barrier detector (), magnetic spectrometer (), and the method of resonant nuclear reaction 15N(p,αγ)12C () Fig. 1 shows the resolving power of scattering methods versus energy losses, as ~ 0.5 MeV protons penetrate deep into the target. The straggling depends PROBLEMS OF ATOMIC SCIENCE AND TECHNOLOGY. 2005, № 6. Series: Nuclear Physics Investigations (45), p. 37-39. 37 on the depth, at which the particle is scattered in the crystal. As it is seen from Fig. 1, in the parts of the proton trajectory before δEin and after δEout scattering in the near-surface zone of the crystal the contribution to the resolving power from straggling is insignificant if a semiconductor-detector spectrometer is used. The measurements of scattered proton energy with the use of a cooled Si - detector (curve ( )) give the worst resolution. This is due to the fact that the semiconductor-detector spectrometer for the protons of this energy has δEspc ~ 9 keV [3]. The use of the magnetic analyzer for the spectrometry of scattered particles [4], as it follows from Fig. 1 ( ), substantially improves the energy resolution. Here the straggling does give a certain contribution to the energy resolution. But in the given case, the magnetic analyzer acts as a differential instrument; besides, its scattered-particle acceptance solid angle is considerably smaller than that of the semiconductor-detector spectrometer. The dependence of the resolving power of the isolated resonance method on the depth, at which the reaction occurs, is defined by the expression ( ) ( ) ( ) ( ) 22222 inDresbmnr EEΓEE δδδ +++=∆ , (2) where δEbm is the beam energy straggling at entry into the crystal, Γres is the natural line width of resonance, δED is the Doppler broadening the natural line with Γres of the resonance, δEin is the energy straggling of particles at entry into the crystal. The resonance can be selected to have Γres > δED. As it follows from Eq. (1), the resolution depends on channeled particle straggling over the part of the trajectory up to the reaction excitation, and is independent of the spectrometer resolution. This enables one to obtain a much better depth resolution by the isolated resonance method rather than by the scattering method. The two methods are equally dependent on δEbm. Stringent requirements are imposed on the technical capabilities of the accelerator. 3. RESULTS AND DISCUSSION The program developed to simulate the channeled particle flux as well as the experimental data on the location of carbon atoms in the single-crystal solution Re-0.4 at.%13C were used to investigate the evolution of proton trajectories in the plane channel (0001) by the isolated resonance method. The nuclear reaction 13C(p,γ)14N, which shows a strong isolated resonance at a proton energy of 1.7476 MeV, Γres = 135 eV, was used to determine the localization of carbon atoms. It has been established [5] that carbon in rhenium occupies octahedral interstitial sites. In crystals with the hexagonal close-packed lattice (rhenium being among them), the plane of octahedral interstitial sites lies just at the center between the (0001) planes. 0,5 1,0 1,5 2,0 0 2 4 6 8 250 200 150 100 50 Plane distance (Å) N or m al iz ed f la x D ep th ( Å ) Fig. 2. Channeled proton flux distribution in the transverse plane along the (0001) channel, E0 = 1.7476 MeV, φin = 0˚ Fig. 2 shows some special features of the dynamic distribution of the proton flux in the (0001) channel up to the first bundle of trajectories for a variety of depth values. As a result of a series of soft correlated collisions with the atoms of the planes, protons having a large amplitude of trajectories give rise to the peaks along the edges of the flux distribution. As the depth grows, the peaks approach the center of the channel and form the maximum in the region of the first bundle of trajectories. As it is obvious from Fig. 1, in the middle of the channel, up to the maximum, the flux of hyperchanneled protons is uniform in the transverse plane, and is close to a constant value, irrespective of the depth value. Fig. 3 shows the calculated (, - - -) and measured ( ) functions of the 13C(p,γ)14N reaction excitation at proton channeling along the (0001) plane up to the first bundle of trajectories. The same figure shows the excitation function for random protons (ÿ ). As 38 expected, a sharp increase in the γ-quantum yield is 1747,5 1748,0 1748,5 1749,0 1749,5 1750,0 0 200 400 600 800 1000 1200 1400 1600 1800 2000 Y ie ld Energy (keV) ↓ Fig. 3. 13C(p,γ)14N reaction yield vs proton energy observed at the resonance energy, irrespective of the beam momentum orientation relative to the crystal. The increase in the reaction yield for random protons attains saturation and further remains unchanged irrespective of energy. The excitation function for channeled protons has a plateau, ~ 400 eV in width (shown by the arrow in the figure). The γ-quantum yield in this region stays close to a constant value, and substantially exceeds the yield from random protons. The hyperchanneled proton flux at the center of the channel, where valence electrons are found (Fig. 1), gives the main contribution to the reaction excitation function in the plateau part. An insignificant contribution to the excitation function comes from dechanneled protons. The increased yield observed in the plateau region as compared to the yield for random protons is accounted for by a decrease in the electron energy losses of hyperchanneled protons on valence electrons. The estimates give the ratio (dE/dx)(0001) / (dE/dx)random to be 0.64. The greatest γ- quantum yield is realized in the region of the first bundle of proton trajectories. The simulation program used here takes into account the thermal vibrations of impurity atoms in the transverse plane of the (0001) channel in the harmonic approximation. Numerical calculations have pointed (Fig. 3) to the existing dependence of the reaction yield at the maximum of the excitation function on the r.m.s. amplitude of thermal vibrations of 13C atoms. As the amplitude of 13C vibrations grows the γ-quantum yield drops. The best agreement between the measured data and the calculations was obtained at the thermal vibration amplitude equal to 0.102 Å. The work was done with partial support of Project X866 ЯMРT 2010. REFERENCES 1. D.S. Gemmell. Channeling and Related Effects in the Motion of Charged Particles Through Crystals // Rev. Mod. Phys. 1974, v. 46, №1, p. 129-227. 2. John H Barrett. Potential and stopping – power information from planar – channeling oscillations // Phys. Rev. 1989, v. 20, №9, p. 3535-3542. 3. F. Abel, G. Amsel, M. Bruneaux, et al. Backscattering study and theoretical investigation of planar channeling processes // Phys. Rev. B. 1975, v. 12, №11 p. 4617-4627. 4. E. Bogh. An application of high energy-resolution scattering measurements in channeling studies // Radiation effects. 1972, v. 12, p. 13-19. 5. N.A. Skakun, V.A. Olejnik et al. Channeling study of carbon atom location in Re – Cx system // Nucl. Instr. Meth. B. 1992, v. 67, p. 199-202. МЕТОД ИЗОЛИРОВАННОГО РЕЗОНАНСА И ЭЛЕКТРОННЫЕ ТОРМОЗНЫЕ ПОТЕРИ ЭНЕРГИИ ГИПЕРКАНАЛИРОВАННЫХ ЧАСТИЦ В.М. Шершнев, Н.А. Скакун Изолированный резонанс ядерной реакции на примесных атомах внедрения использован для изучения ориентационных эффектов. Показано, что этот метод позволяет получить лучшее энергетическое разреше- ние по сравнению с другими методами. Резонанс реакции 13C(p,γ)14N, при энергии протонов 1,7476 МэВ, использовался для исследования распределения потока протонов в плоскостном канале (0001) монокристал- лического раствора Re-0,4 ат.%13С. Установлены особенности выхода γ-квантов реакции в зависимости от энергии. Измерены электронные потери энергии гиперканалированных протонов. Показано, что выход γ- квантов реакции, возбуждаемой каналированными протонами, зависит от амплитуды тепловых колебаний атомов углерода. МЕТОД ІЗОЛЬОВАНОГО РЕЗОНАНСУ ТА ЕЛЕКТРОННІ ГАЛЬМОВІ ВТРАТИ ЕНЕРГІЇ ГІПЕРКАНАЛЬОВАНИХ ЧАСТИНОК В.М. Шершнєв, М.О. Скакун Ізольований резонанс ядерної реакції на впроваджених атомах домішок використано для вивчення орієнтаційних ефектів. Показано, що цей метод дозволяє одержати краще енергетичне розрізнення у порів- нянні з іншими методами. Резонанс реакції 13C(p,γ)14N, при енергії протонів 1,7476 МеВ, використовувався для дослідження розподілу потоку протонів у площинному каналі (0001) монокристалічного розчину Re- 0,4 ат.%13С. Встановлено особливості виходу γ-квантів реакції в залежності від енергії. Виміряно електронні втрати енергії гіперканальованих протонів. Показано, що вихід γ-квантів реакції, що збуджується канальованими протонами, залежить від амплітуди теплових коливань атомів вуглецю. 39 National Science Center “Kharkov Institute of Physics and Technology”, Kharkov, Ukraine Метод изолированного резонанса