Йонообмінні властивості модифікованого силікагелю з закріпленими амідами полігексаметиленгуанідину та малеїнової або о-фталевої кислот

Amides of polyhexamethyleneguanidine and maleic or o-phthalic acids were chemically bound with the silica surface. Adsorption properties of synthesized modified silicas have been studied with respect to V(V)-, Cr(VI)-, Mo(VI)-, and W(VI)-containing anions. Both of adsorbents were found to show high...

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Bibliographic Details
Date:2012
Main Authors: Dadashev, A. D., Tertykh, V. A., Yanovska, E. S., Yanova, K. V.
Format: Article
Language:English
Published: Chuiko Institute of Surface Chemistry National Academy of Sciences of Ukraine 2012
Online Access:https://www.cpts.com.ua/index.php/cpts/article/view/190
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Journal Title:Chemistry, Physics and Technology of Surface

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Chemistry, Physics and Technology of Surface
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Summary:Amides of polyhexamethyleneguanidine and maleic or o-phthalic acids were chemically bound with the silica surface. Adsorption properties of synthesized modified silicas have been studied with respect to V(V)-, Cr(VI)-, Mo(VI)-, and W(VI)-containing anions. Both of adsorbents were found to show high adsorption activity in the acidic and slightly acidic media. Kinetic parameters of the obtained composites are closely similar to a polymeric adsorbent. Reduction of Mo(VI) and Cr(VI) ions was detected at adsorption on silica with bound amide of polyhexamethyleneguanidine and o-phthalic acid. The investigation demonstrates the possibility of the quantitative determination of microamounts of the studied metals in the adsorbent phase using the X-ray-fluorescence analysis after extraction of anions from a solution.