КООРДИНАЦІЙНІ СПОЛУКИ Gd3+ та Dy3+ З ДЕЯКИМИ β-ДИКЕТОНАМИ

New complexes of Dy (III) and Gd (III) with b-diketones containing unsaturated and aryl substituents were synthesized. Metal polymers based on synthesized complexes were obtained by the method of radical polymerization. The composition and structure of synthesized complexes and metal polymers are es...

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Бібліографічні деталі
Дата:2021
Автори: Berezhnytska , Оeksandra, Rohovtsov , Oleksandr, Horbenko , Artur, Fedorov , Yaroslav, Trunova , Olena, Chyhyrynets , Olena, Smola , Sergey
Формат: Стаття
Мова:English
Опубліковано: V.I.Vernadsky Institute of General and Inorganic Chemistry 2021
Онлайн доступ:https://ucj.org.ua/index.php/journal/article/view/324
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Назва журналу:Ukrainian Chemistry Journal

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Ukrainian Chemistry Journal
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spelling oai:ojs2.1444248.nisspano.web.hosting-test.net:article-3242021-08-26T08:45:46Z THE COORDINATION COMPOUNDS Gd (III) AND Dy(III) WITH SOME β-DIKETONES КООРДИНАЦІЙНІ СПОЛУКИ Gd3+ та Dy3+ З ДЕЯКИМИ β-ДИКЕТОНАМИ Berezhnytska , Оeksandra Rohovtsov , Oleksandr Horbenko , Artur Fedorov , Yaroslav Trunova , Olena Chyhyrynets , Olena Smola , Sergey lanthanides, complexes, luminescence properties, metalopolymer, gadolinium, dysprosium, β-diketones. New complexes of Dy (III) and Gd (III) with b-diketones containing unsaturated and aryl substituents were synthesized. Metal polymers based on synthesized complexes were obtained by the method of radical polymerization. The composition and structure of synthesized complexes and metal polymers are established. It is shown that during polymerization the coordination environment of the central ion remains unchanged. The spectral-luminescent cha­racteristics of the synthesized compounds were studied. The presence of water molecules in the immediate coordination environment causes a low intensity of emission of monomeric dysprosium complexes. In the luminescence spectra of metal polymers, there are bands magnetic dipole transition (4F9 → 6H15/2) and electric dipole transition (4F9 → 6H13/2). The close energies of the triplet level of the ligand and the resonant level of the dysprosium ion cause low emission characteristics of the synthesized dysprosium complexes. V.I.Vernadsky Institute of General and Inorganic Chemistry 2021-07-26 Article Article Inorganic Chemistry Неорганическая химия Неорганічна хімія application/pdf https://ucj.org.ua/index.php/journal/article/view/324 10.33609/2708-129X.87.06.2021.97-120 Ukrainian Chemistry Journal; Vol 87 No 6 (2021): Ukrainian Chemistry Journal; 97-120 Украинский химический журнал; Том 87 № 6 (2021): Ukrainian Chemistry Journal; 97-120 Український хімічний журнал; Том 87 № 6 (2021): Український хімічний журнал; 97-120 2708-129X 2708-1281 en https://ucj.org.ua/index.php/journal/article/view/324/175
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datestamp_date 2021-08-26T08:45:46Z
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language English
topic_facet lanthanides
complexes
luminescence properties
metalopolymer
gadolinium
dysprosium
β-diketones.
format Article
author Berezhnytska , Оeksandra
Rohovtsov , Oleksandr
Horbenko , Artur
Fedorov , Yaroslav
Trunova , Olena
Chyhyrynets , Olena
Smola , Sergey
spellingShingle Berezhnytska , Оeksandra
Rohovtsov , Oleksandr
Horbenko , Artur
Fedorov , Yaroslav
Trunova , Olena
Chyhyrynets , Olena
Smola , Sergey
КООРДИНАЦІЙНІ СПОЛУКИ Gd3+ та Dy3+ З ДЕЯКИМИ β-ДИКЕТОНАМИ
author_facet Berezhnytska , Оeksandra
Rohovtsov , Oleksandr
Horbenko , Artur
Fedorov , Yaroslav
Trunova , Olena
Chyhyrynets , Olena
Smola , Sergey
author_sort Berezhnytska , Оeksandra
title КООРДИНАЦІЙНІ СПОЛУКИ Gd3+ та Dy3+ З ДЕЯКИМИ β-ДИКЕТОНАМИ
title_short КООРДИНАЦІЙНІ СПОЛУКИ Gd3+ та Dy3+ З ДЕЯКИМИ β-ДИКЕТОНАМИ
title_full КООРДИНАЦІЙНІ СПОЛУКИ Gd3+ та Dy3+ З ДЕЯКИМИ β-ДИКЕТОНАМИ
title_fullStr КООРДИНАЦІЙНІ СПОЛУКИ Gd3+ та Dy3+ З ДЕЯКИМИ β-ДИКЕТОНАМИ
title_full_unstemmed КООРДИНАЦІЙНІ СПОЛУКИ Gd3+ та Dy3+ З ДЕЯКИМИ β-ДИКЕТОНАМИ
title_sort координаційні сполуки gd3+ та dy3+ з деякими β-дикетонами
title_alt THE COORDINATION COMPOUNDS Gd (III) AND Dy(III) WITH SOME β-DIKETONES
description New complexes of Dy (III) and Gd (III) with b-diketones containing unsaturated and aryl substituents were synthesized. Metal polymers based on synthesized complexes were obtained by the method of radical polymerization. The composition and structure of synthesized complexes and metal polymers are established. It is shown that during polymerization the coordination environment of the central ion remains unchanged. The spectral-luminescent cha­racteristics of the synthesized compounds were studied. The presence of water molecules in the immediate coordination environment causes a low intensity of emission of monomeric dysprosium complexes. In the luminescence spectra of metal polymers, there are bands magnetic dipole transition (4F9 → 6H15/2) and electric dipole transition (4F9 → 6H13/2). The close energies of the triplet level of the ligand and the resonant level of the dysprosium ion cause low emission characteristics of the synthesized dysprosium complexes.
publisher V.I.Vernadsky Institute of General and Inorganic Chemistry
publishDate 2021
url https://ucj.org.ua/index.php/journal/article/view/324
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