STRUCTURE AND SPECTRAL-LUMUINESCENT PROPERTIES OF LANTHANIDE-CONTAINING COMPLEXES WITH AZACROWN CALIXARENES

Lanthanide complexes with calix[4]arenes lower rim substituted with two azacrown ether fragments are reported. The size of the substituent cavity varied from 4 to 6 heteroatoms. The complexes were analyzed by means of IR, NMR, ESI mass spectroscopy. It is assumed that the coordination of Ln(III) ion...

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Datum:2021
Hauptverfasser: Smola, Serhii, Rusakova, Natalia, Alekseeva, Olena, Basok, Stepan, Kirichenko, Tatiana, Korovin, Oleksandr, Malinka, Olena, Semenishyn, Nikolay
Format: Artikel
Sprache:English
Veröffentlicht: V.I.Vernadsky Institute of General and Inorganic Chemistry 2021
Online Zugang:https://ucj.org.ua/index.php/journal/article/view/372
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Назва журналу:Ukrainian Chemistry Journal

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Ukrainian Chemistry Journal
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Zusammenfassung:Lanthanide complexes with calix[4]arenes lower rim substituted with two azacrown ether fragments are reported. The size of the substituent cavity varied from 4 to 6 heteroatoms. The complexes were analyzed by means of IR, NMR, ESI mass spectroscopy. It is assumed that the coordination of Ln(III) ions occurs through the donor atoms of the lower rim; the counter anion and solvent molecule are also coordinated. Lanthanide-centered characteristic luminescence was observed in Eu(III), Tb(III) and Yb(III) complexes. The most efficient 4f-luminescence is observed for terbium-containing complexes with benzo-crown-derived ligands. The pathways of the sensitization of 4f-luminescence are discussed.