INFLUENCE OF CLAY MINERAL ADDITIVES ON THE PROPERTIES OF COMPOSITE WATER–COAL FUEL.

The study aimed to examine the electrokinetic and rheological properties of composite water-coal fuel (CWCF) based on anthracite and P-grade coal in the presence of clay mi­nerals. The influence of clay mineral additives on the electrokinetic and rheological properties of CWCF was studied. The clay...

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Datum:2023
Hauptverfasser: Klishchenko, Roman, Kornienko, Ivan, Shkutkova, Olena
Format: Artikel
Sprache:English
Veröffentlicht: V.I.Vernadsky Institute of General and Inorganic Chemistry 2023
Online Zugang:https://ucj.org.ua/index.php/journal/article/view/613
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Назва журналу:Ukrainian Chemistry Journal

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Ukrainian Chemistry Journal
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spelling oai:ojs2.1444248.nisspano.web.hosting-test.net:article-6132024-10-07T12:25:33Z INFLUENCE OF CLAY MINERAL ADDITIVES ON THE PROPERTIES OF COMPOSITE WATER–COAL FUEL. Klishchenko, Roman Kornienko, Ivan Shkutkova, Olena composite water-coal fuel, anthracite, P-grade coal, montmorillonite, illite, kaolinite. The study aimed to examine the electrokinetic and rheological properties of composite water-coal fuel (CWCF) based on anthracite and P-grade coal in the presence of clay mi­nerals. The influence of clay mineral additives on the electrokinetic and rheological properties of CWCF was studied. The clay minerals used were montmorillonite, illite, and kaoli­nite from Ukrainian deposits. The fuel was prepared based on P-grade coal and anthracite. The share of the solid phase (coal) in the suspensions was 62 %. According to the particle size distribution, the bulk of the coal has a size of 30–110 μm with a bimodal distribution. To obtain the CWCF, the coal powder was homogenized with the dispersion medium by wet grinding in a ball mill for 20–25 minutes. The dispersion medium was distilled water. Wet grinding was carried out until particles < 0.25 mm in size were obtained. We obtained a CWCF with a concentration of 62% of the so­lid phase of coal. Additions of chemicals were not practiced to study the effect of clay mine­rals in a pure experiment. Clay minerals were added at a concentration of 0.5–3 % by weight of the CWCFs. Their rheological data were measured using a Rheotest-2 rheometer at a temperature of 20 ºC and the shear-stress/shear-rate data for the CWCF covered a range of 0.1 to 470 s-1.  The sedimentation stability of St was stu­died at the time of stratification of the CWCF sample in a measuring cylinder. After preparation, a 10-mL sample of the CWCF was placed in a 25-mL glass cylinder. St is equal to the time of the beginning of the suspension stratification in days. It was established that ξ - the potential of CWCF particles with the addition of clay mine­rals shifts to the negative region and reaches – 45–50 mV at pH>8. Montmorillonite was found to be most effective additive for controlling the properties of the CWCF. Systems with clay mineral additives demonstrate a pseudoplastic type of flow in the range of shear rates γ 0–100 s-1 and a Newtonian type of flow at higher γ. According to their effect on the increase in apparent viscosity, clay mine­rals are arranged in the following order: kaolinite, illite, and montmorillonite. The thixotropic properties of the studied systems provide complete restoration of the properties of the CWCF when the shear rate is reduced to 0–40 s-1. Sedimentation stability in the presence of illite and montmorillonite additives reaches 8–14 days. In contrast to illite and montmorillonite, kaolinite has a very weak effect on the properties of CWCF. V.I.Vernadsky Institute of General and Inorganic Chemistry 2023-12-29 Article Article Physical chemistry Физическая xимия Фізична xімія application/pdf https://ucj.org.ua/index.php/journal/article/view/613 10.33609/2708-129X.89.11.2023.35-50 Ukrainian Chemistry Journal; Vol. 89 No. 11 (2023): Ukrainian Chemistry Journal; 35-50 Украинский химический журнал; Том 89 № 11 (2023): Ukrainian Chemistry Journal; 35-50 Український хімічний журнал; Том 89 № 11 (2023): Український хімічний журнал; 35-50 2708-129X 2708-1281 en https://ucj.org.ua/index.php/journal/article/view/613/308
institution Ukrainian Chemistry Journal
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datestamp_date 2024-10-07T12:25:33Z
collection OJS
language English
topic_facet composite water-coal fuel
anthracite
P-grade coal
montmorillonite
illite
kaolinite.
format Article
author Klishchenko, Roman
Kornienko, Ivan
Shkutkova, Olena
spellingShingle Klishchenko, Roman
Kornienko, Ivan
Shkutkova, Olena
INFLUENCE OF CLAY MINERAL ADDITIVES ON THE PROPERTIES OF COMPOSITE WATER–COAL FUEL.
author_facet Klishchenko, Roman
Kornienko, Ivan
Shkutkova, Olena
author_sort Klishchenko, Roman
title INFLUENCE OF CLAY MINERAL ADDITIVES ON THE PROPERTIES OF COMPOSITE WATER–COAL FUEL.
title_short INFLUENCE OF CLAY MINERAL ADDITIVES ON THE PROPERTIES OF COMPOSITE WATER–COAL FUEL.
title_full INFLUENCE OF CLAY MINERAL ADDITIVES ON THE PROPERTIES OF COMPOSITE WATER–COAL FUEL.
title_fullStr INFLUENCE OF CLAY MINERAL ADDITIVES ON THE PROPERTIES OF COMPOSITE WATER–COAL FUEL.
title_full_unstemmed INFLUENCE OF CLAY MINERAL ADDITIVES ON THE PROPERTIES OF COMPOSITE WATER–COAL FUEL.
title_sort influence of clay mineral additives on the properties of composite water–coal fuel.
description The study aimed to examine the electrokinetic and rheological properties of composite water-coal fuel (CWCF) based on anthracite and P-grade coal in the presence of clay mi­nerals. The influence of clay mineral additives on the electrokinetic and rheological properties of CWCF was studied. The clay minerals used were montmorillonite, illite, and kaoli­nite from Ukrainian deposits. The fuel was prepared based on P-grade coal and anthracite. The share of the solid phase (coal) in the suspensions was 62 %. According to the particle size distribution, the bulk of the coal has a size of 30–110 μm with a bimodal distribution. To obtain the CWCF, the coal powder was homogenized with the dispersion medium by wet grinding in a ball mill for 20–25 minutes. The dispersion medium was distilled water. Wet grinding was carried out until particles < 0.25 mm in size were obtained. We obtained a CWCF with a concentration of 62% of the so­lid phase of coal. Additions of chemicals were not practiced to study the effect of clay mine­rals in a pure experiment. Clay minerals were added at a concentration of 0.5–3 % by weight of the CWCFs. Their rheological data were measured using a Rheotest-2 rheometer at a temperature of 20 ºC and the shear-stress/shear-rate data for the CWCF covered a range of 0.1 to 470 s-1.  The sedimentation stability of St was stu­died at the time of stratification of the CWCF sample in a measuring cylinder. After preparation, a 10-mL sample of the CWCF was placed in a 25-mL glass cylinder. St is equal to the time of the beginning of the suspension stratification in days. It was established that ξ - the potential of CWCF particles with the addition of clay mine­rals shifts to the negative region and reaches – 45–50 mV at pH>8. Montmorillonite was found to be most effective additive for controlling the properties of the CWCF. Systems with clay mineral additives demonstrate a pseudoplastic type of flow in the range of shear rates γ 0–100 s-1 and a Newtonian type of flow at higher γ. According to their effect on the increase in apparent viscosity, clay mine­rals are arranged in the following order: kaolinite, illite, and montmorillonite. The thixotropic properties of the studied systems provide complete restoration of the properties of the CWCF when the shear rate is reduced to 0–40 s-1. Sedimentation stability in the presence of illite and montmorillonite additives reaches 8–14 days. In contrast to illite and montmorillonite, kaolinite has a very weak effect on the properties of CWCF.
publisher V.I.Vernadsky Institute of General and Inorganic Chemistry
publishDate 2023
url https://ucj.org.ua/index.php/journal/article/view/613
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