Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers

Multifractal analysis is performed for description of the surface topography of thin polycrystalline gold film. Its structure was modified by annealing at different temperatures in the range 20÷200 ⁰C and films were imaged by Atomic Force Microscopy. Image was analyzed as a collection of layers take...

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Veröffentlicht in:Semiconductor Physics Quantum Electronics & Optoelectronics
Datum:1999
Hauptverfasser: Snopoka, B., Strizhak, P., Kostyukevich, E., Serebriy, V., Lysenko, S., Shepeliavii, P., Priatkin, S.L., Kostuykevich, S., Shirshov, Yu., Venger, E.
Format: Artikel
Sprache:English
Veröffentlicht: Інститут фізики напівпровідників імені В.Є. Лашкарьова НАН України 1999
Online Zugang:https://nasplib.isofts.kiev.ua/handle/123456789/119875
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Назва журналу:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Zitieren:Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers / B. Snopok, P. Strizhak, E. Kostyukevicha, V. Serebriy, S. Lysenko, P. Shepeliavii, S.L. Priatkin, S. Kostuykevich, Yu. Shirshov, E. Venger // Semiconductor Physics Quantum Electronics & Optoelectronics. — 1999. — Т. 2, № 3. — С. 86-97. — Бібліогр.: 30 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
id nasplib_isofts_kiev_ua-123456789-119875
record_format dspace
spelling Snopoka, B.
Strizhak, P.
Kostyukevich, E.
Serebriy, V.
Lysenko, S.
Shepeliavii, P.
Priatkin, S.L.
Kostuykevich, S.
Shirshov, Yu.
Venger, E.
2017-06-10T08:07:43Z
2017-06-10T08:07:43Z
1999
Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers / B. Snopok, P. Strizhak, E. Kostyukevicha, V. Serebriy, S. Lysenko, P. Shepeliavii, S.L. Priatkin, S. Kostuykevich, Yu. Shirshov, E. Venger // Semiconductor Physics Quantum Electronics & Optoelectronics. — 1999. — Т. 2, № 3. — С. 86-97. — Бібліогр.: 30 назв. — англ.
1560-8034
PACS: 61.66.Hq, 61.43.Hv, 61.72.Cc, 68.35.Bs, 68.35.Rh, 67.70.+n, 81.65.Ya
https://nasplib.isofts.kiev.ua/handle/123456789/119875
Multifractal analysis is performed for description of the surface topography of thin polycrystalline gold film. Its structure was modified by annealing at different temperatures in the range 20÷200 ⁰C and films were imaged by Atomic Force Microscopy. Image was analyzed as a collection of layers taken parallel to the mean surface. Fractal subsets with different scaling properties were described by multifractal divergence (e.g. the difference between maximal and minimal values of the f (a) spectrum). This allowed to highlight the effect of the temperature of film annealing on the surface structure. We found that fractal diversity jumps down in the temperature range 130÷140 ⁰C. Therefore, phase transition occurs in the system. Below the temperature of the phase transition the surface topography is characterized by high roughness and existence of small-scale irregularities. At critical temperature the surface structure undergoes morphological transition caused by melting of small-scale irregularities. The melting also results in a decrease of the surface roughness due to the flowing down of gold crystallites. A notable feature of the approach is its ability to highlight a possible influence of substrate structure on the adsorption/self-assembling processes at the interface, which may be disturbed by the surface irregularities. The typical and expressive example taken from the self-assembling on the polycrystalline substrate. Particularly, substrate topography determines an order of thiols layers resulting in peculiarities of chemical functionality of obtained material. It was shown that formation of well-ordered monolayers of ω-substituted alkanethiols on gold films occurs only if the freshly evaporated gold films were annealed at temperature more than ca.120 ⁰C. The analysis of surface peculiarities allows suggesting that this behavior is caused by disappearance of short-scale multifractal structures. Therefore, the multifractal analysis opens a new avenue for both characterization and direct prediction of surface properties. Particularly, it gives a hint regarding a formation of the Euclidean two-imensional structures at the multifractal substrates.
en
Інститут фізики напівпровідників імені В.Є. Лашкарьова НАН України
Semiconductor Physics Quantum Electronics & Optoelectronics
Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers
Article
published earlier
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
title Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers
spellingShingle Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers
Snopoka, B.
Strizhak, P.
Kostyukevich, E.
Serebriy, V.
Lysenko, S.
Shepeliavii, P.
Priatkin, S.L.
Kostuykevich, S.
Shirshov, Yu.
Venger, E.
title_short Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers
title_full Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers
title_fullStr Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers
title_full_unstemmed Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers
title_sort interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers
author Snopoka, B.
Strizhak, P.
Kostyukevich, E.
Serebriy, V.
Lysenko, S.
Shepeliavii, P.
Priatkin, S.L.
Kostuykevich, S.
Shirshov, Yu.
Venger, E.
author_facet Snopoka, B.
Strizhak, P.
Kostyukevich, E.
Serebriy, V.
Lysenko, S.
Shepeliavii, P.
Priatkin, S.L.
Kostuykevich, S.
Shirshov, Yu.
Venger, E.
publishDate 1999
language English
container_title Semiconductor Physics Quantum Electronics & Optoelectronics
publisher Інститут фізики напівпровідників імені В.Є. Лашкарьова НАН України
format Article
description Multifractal analysis is performed for description of the surface topography of thin polycrystalline gold film. Its structure was modified by annealing at different temperatures in the range 20÷200 ⁰C and films were imaged by Atomic Force Microscopy. Image was analyzed as a collection of layers taken parallel to the mean surface. Fractal subsets with different scaling properties were described by multifractal divergence (e.g. the difference between maximal and minimal values of the f (a) spectrum). This allowed to highlight the effect of the temperature of film annealing on the surface structure. We found that fractal diversity jumps down in the temperature range 130÷140 ⁰C. Therefore, phase transition occurs in the system. Below the temperature of the phase transition the surface topography is characterized by high roughness and existence of small-scale irregularities. At critical temperature the surface structure undergoes morphological transition caused by melting of small-scale irregularities. The melting also results in a decrease of the surface roughness due to the flowing down of gold crystallites. A notable feature of the approach is its ability to highlight a possible influence of substrate structure on the adsorption/self-assembling processes at the interface, which may be disturbed by the surface irregularities. The typical and expressive example taken from the self-assembling on the polycrystalline substrate. Particularly, substrate topography determines an order of thiols layers resulting in peculiarities of chemical functionality of obtained material. It was shown that formation of well-ordered monolayers of ω-substituted alkanethiols on gold films occurs only if the freshly evaporated gold films were annealed at temperature more than ca.120 ⁰C. The analysis of surface peculiarities allows suggesting that this behavior is caused by disappearance of short-scale multifractal structures. Therefore, the multifractal analysis opens a new avenue for both characterization and direct prediction of surface properties. Particularly, it gives a hint regarding a formation of the Euclidean two-imensional structures at the multifractal substrates.
issn 1560-8034
url https://nasplib.isofts.kiev.ua/handle/123456789/119875
citation_txt Interfacial architecture on the fractal support: polycrystalline gold films as support for self-assembling monolayers / B. Snopok, P. Strizhak, E. Kostyukevicha, V. Serebriy, S. Lysenko, P. Shepeliavii, S.L. Priatkin, S. Kostuykevich, Yu. Shirshov, E. Venger // Semiconductor Physics Quantum Electronics & Optoelectronics. — 1999. — Т. 2, № 3. — С. 86-97. — Бібліогр.: 30 назв. — англ.
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AT serebriyv interfacialarchitectureonthefractalsupportpolycrystallinegoldfilmsassupportforselfassemblingmonolayers
AT lysenkos interfacialarchitectureonthefractalsupportpolycrystallinegoldfilmsassupportforselfassemblingmonolayers
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