Large-area surface wave plasma source

A surface wave plasma source for the production of a large-diameter, high electron density and low electron temperature plasma at low pressure without using a magnetic field for plasma processing and thin film preparation are. The DC or RF voltage with the frequency of 13.56 MHz can supply the sourc...

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Veröffentlicht in:Вопросы атомной науки и техники
Datum:2002
Hauptverfasser: Azarenkov, N.A., Bizyukov, A.A., Sereda, K.N., Tseluyko, A.Ph., Yunakov, N.N., Gapon, A.V., Kashaba, A.Y.
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Sprache:English
Veröffentlicht: Національний науковий центр «Харківський фізико-технічний інститут» НАН України 2002
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Online Zugang:https://nasplib.isofts.kiev.ua/handle/123456789/79286
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Zitieren:Large-area surface wave plasma source / N.A. Azarenkov, A.A. Bizyukov, A.V. Gapon, A.Y. Kashaba, K.N. Sereda, A.Ph. Tseluyko, N.N. Yunakov // Вопросы атомной науки и техники. — 2002. — № 5. — С. 118-120. — Бібліогр.: 6 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
id nasplib_isofts_kiev_ua-123456789-79286
record_format dspace
spelling Azarenkov, N.A.
Bizyukov, A.A.
Sereda, K.N.
Tseluyko, A.Ph.
Yunakov, N.N.
Gapon, A.V.
Kashaba, A.Y.
2015-03-30T09:37:26Z
2015-03-30T09:37:26Z
2002
Large-area surface wave plasma source / N.A. Azarenkov, A.A. Bizyukov, A.V. Gapon, A.Y. Kashaba, K.N. Sereda, A.Ph. Tseluyko, N.N. Yunakov // Вопросы атомной науки и техники. — 2002. — № 5. — С. 118-120. — Бібліогр.: 6 назв. — англ.
1562-6016
PACS: 52.50.Dg
https://nasplib.isofts.kiev.ua/handle/123456789/79286
A surface wave plasma source for the production of a large-diameter, high electron density and low electron temperature plasma at low pressure without using a magnetic field for plasma processing and thin film preparation are. The DC or RF voltage with the frequency of 13.56 MHz can supply the source. The pumping-out of the source is carried out through the insulated substrate holder. The plasma source operates in a working gas pressure range of 3∙10⁻² ÷ 10⁻⁴ Torr with changing the RF power in a range of 50÷1000 W during the discharge on surface waves with the mode 0 excited by a ring antenna. The plasma density has a homogeneous distribution over a diameter of 300 mm and varies in a range of 10⁸÷10¹⁰ cm⁻³ at electron temperature of 2÷7 eV depending on external parameters. An ion beam density in the presence of the RF bias applied to the substrate holder reached 0.1 mA/сm² with homogeneous distribution over the diameter of 300 mm. The total ion current to the substrate holder with a diameter of 467 mm reaches the value of 2 A with average ion energy of 200 eV. Numerical analysis of electric field distribution over the processing chamber in linear approach was made and compared to experimental results obtained.
This work was supported by Scientific Technical Centre of Ukraine, Project #1112.
en
Національний науковий центр «Харківський фізико-технічний інститут» НАН України
Вопросы атомной науки и техники
Low temperature plasma and plasma technologies
Large-area surface wave plasma source
Article
published earlier
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
title Large-area surface wave plasma source
spellingShingle Large-area surface wave plasma source
Azarenkov, N.A.
Bizyukov, A.A.
Sereda, K.N.
Tseluyko, A.Ph.
Yunakov, N.N.
Gapon, A.V.
Kashaba, A.Y.
Low temperature plasma and plasma technologies
title_short Large-area surface wave plasma source
title_full Large-area surface wave plasma source
title_fullStr Large-area surface wave plasma source
title_full_unstemmed Large-area surface wave plasma source
title_sort large-area surface wave plasma source
author Azarenkov, N.A.
Bizyukov, A.A.
Sereda, K.N.
Tseluyko, A.Ph.
Yunakov, N.N.
Gapon, A.V.
Kashaba, A.Y.
author_facet Azarenkov, N.A.
Bizyukov, A.A.
Sereda, K.N.
Tseluyko, A.Ph.
Yunakov, N.N.
Gapon, A.V.
Kashaba, A.Y.
topic Low temperature plasma and plasma technologies
topic_facet Low temperature plasma and plasma technologies
publishDate 2002
language English
container_title Вопросы атомной науки и техники
publisher Національний науковий центр «Харківський фізико-технічний інститут» НАН України
format Article
description A surface wave plasma source for the production of a large-diameter, high electron density and low electron temperature plasma at low pressure without using a magnetic field for plasma processing and thin film preparation are. The DC or RF voltage with the frequency of 13.56 MHz can supply the source. The pumping-out of the source is carried out through the insulated substrate holder. The plasma source operates in a working gas pressure range of 3∙10⁻² ÷ 10⁻⁴ Torr with changing the RF power in a range of 50÷1000 W during the discharge on surface waves with the mode 0 excited by a ring antenna. The plasma density has a homogeneous distribution over a diameter of 300 mm and varies in a range of 10⁸÷10¹⁰ cm⁻³ at electron temperature of 2÷7 eV depending on external parameters. An ion beam density in the presence of the RF bias applied to the substrate holder reached 0.1 mA/сm² with homogeneous distribution over the diameter of 300 mm. The total ion current to the substrate holder with a diameter of 467 mm reaches the value of 2 A with average ion energy of 200 eV. Numerical analysis of electric field distribution over the processing chamber in linear approach was made and compared to experimental results obtained.
issn 1562-6016
url https://nasplib.isofts.kiev.ua/handle/123456789/79286
citation_txt Large-area surface wave plasma source / N.A. Azarenkov, A.A. Bizyukov, A.V. Gapon, A.Y. Kashaba, K.N. Sereda, A.Ph. Tseluyko, N.N. Yunakov // Вопросы атомной науки и техники. — 2002. — № 5. — С. 118-120. — Бібліогр.: 6 назв. — англ.
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AT bizyukovaa largeareasurfacewaveplasmasource
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AT yunakovnn largeareasurfacewaveplasmasource
AT gaponav largeareasurfacewaveplasmasource
AT kashabaay largeareasurfacewaveplasmasource
first_indexed 2025-11-25T21:07:14Z
last_indexed 2025-11-25T21:07:14Z
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fulltext LOW TEMPERATURE PLASMA AND PLASMA TECHNOLOGIES LARGE-AREA SURFACE WAVE PLASMA SOURCE N.A. Azarenkov, A.A. Bizyukov, A.V. Gapon, A.Y. Kashaba, K.N. Sereda, A.Ph. Tseluyko, N.N. Yunakov Kharkiv National University, Kharkiv, Ukraine, 61108, E-mail: bizyukov@pht.univer.kharkov.ua A surface wave plasma source for the production of a large-diameter, high electron density and low electron temperature plasma at low pressure without using a magnetic field for plasma processing and thin film preparation are. The DC or RF voltage with the frequency of 13.56 MHz can supply the source. The pumping-out of the source is carried out through the insulated substrate holder. The plasma source operates in a working gas pressure range of Torr42 10103 −− ÷⋅ with changing the RF power in a range of 50÷1000 W during the discharge on surface waves with the mode 0 excited by a ring antenna. The plasma density has a homogeneous distribution over a diameter of 300 mm and varies in a range of 108÷1010 cm-3 at electron temperature of 2÷7 eV depending on external parameters. An ion beam density in the presence of the RF bias applied to the substrate holder reached 0.1 mA/сm2 with homogeneous distribution over the diameter of 300 mm. The total ion current to the substrate holder with a diameter of 467 mm reaches the value of 2 A with average ion energy of 200 eV. Numerical analysis of electric field distribution over the processing chamber in linear approach was made and compared to experimental results obtained. PACS: 52.50.Dg 1. INTRODUCTION Low pressure (less than 10 mTorr), high-density (more than 109 cm-3) plasma sources which produce uniform (less than 5%) densities of ions and radicals over large areas (more than 300 mm diameter) have recently been important for plasma etching and deposition technology in the fabrication of ultralarge-scale integrated (ULSI) circuits with deep submicron features [1, 2]. Among the various types of plasmas (inductively coupled plasma (ICP), electron cyclotron resonance (ECR) plasma, helicon, etc. [3] ), surface-wave plasmas (SWPs) are one of the most promising candidates from the viewpoints of cost performance, compactness and feasibility of enlargment of high density homogeneous plasmas [4]. This paper presents a surface wave plasma source for the production of high-density plasma over large areas without a magnetic field for plasma processing and thin film preparation. Fig. 1. Schematic diagram of the plasma source. 1 – housing ; 2-flat ring electrode; 3, 4 – dielectric plates; 5 – cylindrical ring electrode; 6 – gridded electrode, 7 – substrate holder 2. EXPERIMENTAL The plasma source consists of a cylindrical housing made of stainless steel, flat and cylindrical ring electrodes, two round flat dielectric plates, high-frequency electrical vacuum lead-ins, insulated substrate holder. The internal diameter of the housing is 505 mm, height is 215 mm, thickness of end wall is 10 mm. The flat ring electrode, which geometrical sizes can vary, is placed on the interior side of the end wall between two round flat dielectric plates with the diameter of 502 mm and thickness of 4 mm. The cylindrical ring electrode with an internal diameter of 492 mm and height of 80 mm has a wall thickness of 3 mm and is arranged coaxially to the housing near the end wall. Both flat, and the cylindrical ring electrodes with excitation of surface waves with different modes can serve as antenna. The insulated substrate holder with the maximum diameter of 498 mm is arranged on an opposite end of the housing. In some experiments, to extract the ions from the discharge volume the gridded electrode with a diameter of 460 mm made stainless steel is disposed from above of the cylindrical electrode. The transparency of the gridded electrode is approximately 50%. The distance between the end of the cylindrical electrode and gridded electrode can also vary from 0 up to 100 mm. The DC or RF voltage with the frequency of 13.56 MHz can be supplied to flat or cylindrical ring electrodes. The plasma source is mounted on the modernized vacuum chamber of base vacuum installation such as UVN which allows to perform preliminary source evacuation to residual pressure 5×10-6 Torr. The gas inlet system allows to support working gas pressure in range of 10-1÷10-5 Torr. 118 Problems of Atomic Science and Technology. 2002. №5. Series: Plasma Physics (8). P. 118-120 3. RESULTS AND DISCUSSION The plasma source operates in a working gas pressure range of Torr42 10103 −− ÷⋅ with changing the RF power in a range of 50÷1000 W during the discharge on surface waves with the mode 0 excited by a flat ring electrode- antenna. In the selected geometry the conditions are suitable for launching of the surface wave sustained discharge. The probe measurements indicate that the plasma density has a homogeneous distribution over a diameter of 300 mm and varies in a range of 108÷1010 cm-3 at electron temperature of 2÷7 eV depending on external parameters. Fig 2. shows plasma density distribution and electron temperature along radial direction of the system. Fig 3. shows dependence of plasma density and electron temperature on the input power. An ion beam density in the presence of the RF bias applied to the substrate holder, which was studied by the system of flat directional probes, reached 0.1 mA/сm2 with homogeneous distribution over the diameter of 300 mm. In the case of applying the positive DC bias to the cylindrical electrode, the dependencies of ion current to the substrate holder at typical external working parameters of the plasma source has linear character within the range of DC bias from 0 to 1000 V. The spatial distribution of ion current density is homogeneous over a diameter of 300 mm. The total ion current to the substrate holder with a diameter of 467 mm reaches the value of 2 A with average ion energy of 200 eV. The carbon films with the evident diamond-like properties was synthesized on the glassceramic substrate surface from a mixture of cyclohexane and hydrogen. The calculation of an RF-field was carried out using the configuration similar to the planar reactor. In spite of the fact that an electric field is enough for ionization maintenance, the linear approach is traditional for amplitude distribution calculation and dispersion characteristics [4 - 6]. Since length of an electromagnetic wave in vacuum for used frequency m10∝λ for frequency wave 13.56 MHz a quasistationary condition was satisfied ( L> >λ , L - the size of considered region) and one can consider that electric field is potential. Considering that the time dependence of unknown fields ),( tru  is specified by applied RF field as )exp()(),( tirUtru ω  = (cyclic frequency π νω 2= , where ν - the generator frequency), the equation for an RF-potential can be written in the following view: Q vt πψ ω ψε 4)( 4 2 2 −=∇+∇∇ , (1) where )( 1 2 coll p iνωω ω ε + −= - plasma permittivity, Q - extraneous charge density, collν - effective electron collision frequency. The regional conditions were chosen as in ref. [6]: 02 2 2 =        −∇∇ S p t p p v n ψ ω ψ  , (2) 0=∇−∇ Sddp nn ψεψ  , (3) where n  - normal line to an interface S, pψ - RF potential in plasma, dψ - potential in a dielectric. The solution was found numerically using finite- difference equations obtained by a method of the streams [6]. Fig. 4 shows the potential distribution normalized by peak value for conditions similar to experimental one. The plasma permittivity varies in range from minimum value –100 up to the 1 near the boundary. Potential reaches the greatest value on the surface where the plasma resonance condition is satisfied. Far from the antenna the potential distribution is nearly the natural solution of the equation (1). The significant voltage dropping toward the axis is distinct that has been found out experimentally. Taking into account electron pressure here is essential. The identical potential profile was calculated using cold plasma approach and is shown in Fig. 5 for comparison with previous one. 0 4 8 12 16 20 24 0 2 4 6 n i r , см T e , эВ 0 2 4 6 T e n i × 10 8 , см -3 0 100 200 300 4 6 8 10 ВЧ-мощность, Вт T e , эВ 0 2 4 6 n i T e n i × 10 8 , см -3 Fig 2. Ion density and electron temperature distribution along radial direction of the system. 3102 −⋅=p Torr, 100=RFP W, working gas was argon Fig. 3. Dependencies of plasma density and electron temperature on the input power. 3102 −⋅=p Torr, working gas was argon 119 Fig. 4. Electron temperature Te=5 eV, distance between glass disks d=3 cm, ro=20 cm, zo=0.4 cm Fig. 5. Cold plasma approach. Geometrical factors see on caption for Fig.4 4. CONCLUSIONS A surface wave plasma source for the production of a large-diameter, high electron density and low electron temperature plasma at low pressure without using a magnetic field for plasma processing and thin film preparation are. The DC or RF voltage with the frequency of 13.56 MHz can supply the source. Numerical analysis of electric field distribution over the processing chamber in linear approach was made and compared to experimental results obtained. 5. ACKNOWLEDGMENTS This work was supported by Scientific Technical Centre of Ukraine, Project #1112. REFERENCES 1.ULSI Technology, ed. C.Y. Chang and S.M. Sze, New York: «Mc Graw-Hill», 1996. 2.M.A. Lieberman, A.J. Lichtenberg, Principles of Plasma Discharges and Materials Processing, New York, «Wiley-Interscience», 1994. 3.High Density Plasma Sources, Design, Physics and Performance, ed. O.A. Popov, New York, «Noyes Publication», 1995. 4.Microwave Discharges, Fundamentals and Applications, eds. C.M. Ferreira and M. Moisan, Nato ASI Series, Series B, Physics 302, New York, London, «Plenum Press», 1993. 5.A.N.Kondratenko. Surface and volumetric waves in bounded plasma. Moscow, Energoatomizdat, 1985, p.207(in Russian). 6.Kroll N., Trajvelpis A. Basics of Plasma Physics, (Transl. From English), Мoscow, Mir, 1975, p.525. 120 E-mail: bizyukov@pht.univer.kharkov.ua References